4,4'''-dichloro-5',5''-bis(1-pyrrolidinylmethyl)<1,1':3',1'':3'',1'''-quaterphenyl>-4'',6'-diol

Base Information

Chemical Name:4,4'''-dichloro-5',5''-bis(1-pyrrolidinylmethyl)<1,1':3',1'':3'',1'''-quaterphenyl>-4'',6'-diol
CAS No.:85842-02-0
Molecular Formula:C₃₄H₃₄Cl₂N₂O₂
Molecular Weight:573.562
Hs Code.:

Synonyms:

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Chemical Property of 4,4'''-dichloro-5',5''-bis(1-pyrrolidinylmethyl)<1,1':3',1'':3'',1'''-quaterphenyl>-4'',6'-diol

Chemical Property:

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Technology Process of 4,4'''-dichloro-5',5''-bis(1-pyrrolidinylmethyl)<1,1':3',1'':3'',1'''-quaterphenyl>-4'',6'-diol

There total 7 articles about 4,4'''-dichloro-5',5''-bis(1-pyrrolidinylmethyl)<1,1':3',1'':3'',1'''-quaterphenyl>-4'',6'-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 123-75-1
pyrrolidine

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 85842-01-9
4,4'''-dichloro<1,1':3',1'':3'',1'''-quaterphenyl>-4'',6'-diol

: 85842-02-0
4,4'''-dichloro-5',5''-bis(1-pyrrolidinylmethyl)<1,1':3',1'':3'',1'''-quaterphenyl>-4'',6'-diol

Guidance literature:: In ethanol; for 2h; Heating; in steal bomb;

Reference yield:

: 85841-96-9
4'-chloro-5-nitro<1,1'-biphenyl>-2-ol

: 85842-02-0
4,4'''-dichloro-5',5''-bis(1-pyrrolidinylmethyl)<1,1':3',1'':3'',1'''-quaterphenyl>-4'',6'-diol

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / NaH / dimethylformamide / 2 h / Heating

2: 100 percent / H₂ / Raney Nickel / ethanol; tetrahydrofuran

3: 1.) water, 0 to 5 deg C, 30 min.; 2.) water

4: 36 percent / activated copper powder / 4 h / 290 °C / in steal bomb

5: 83 percent / boron tribromide / CH₂Cl₂ / 4 h / Ambient temperature

6: 65 percent / ethanol / 2 h / Heating; in steal bomb

With hydrogen; boron tribromide; copper; sodium hydride; nickel; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 85841-97-0
4'-chloro-2-methoxy-5-nitro<1,1'-biphenyl>

: 85842-02-0
4,4'''-dichloro-5',5''-bis(1-pyrrolidinylmethyl)<1,1':3',1'':3'',1'''-quaterphenyl>-4'',6'-diol

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / H₂ / Raney Nickel / ethanol; tetrahydrofuran

2: 1.) water, 0 to 5 deg C, 30 min.; 2.) water

3: 36 percent / activated copper powder / 4 h / 290 °C / in steal bomb

4: 83 percent / boron tribromide / CH₂Cl₂ / 4 h / Ambient temperature

5: 65 percent / ethanol / 2 h / Heating; in steal bomb

With hydrogen; boron tribromide; copper; nickel; In tetrahydrofuran; ethanol; dichloromethane;