trans-[Co(N,N'-bis(pyrrol-2-ylmethylene)-2-aminobenzylamine)(N-methylimidazole)2]BPh₄

Base Information

• Chemical Name: trans-[Co(N,N'-bis(pyrrol-2-ylmethylene)-2-aminobenzylamine)(N-methylimidazole)2]BPh₄
• CAS No.: 1309802-53-6
• Molecular Formula: C₂₄H₂₀B*C₂₅H₂₆CoN₈
• Molecular Weight: 816.762

Synonyms:

Chemical Property of trans-[Co(N,N'-bis(pyrrol-2-ylmethylene)-2-aminobenzylamine)(N-methylimidazole)2]BPh₄

Chemical Property:

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Technology Process of trans-[Co(N,N'-bis(pyrrol-2-ylmethylene)-2-aminobenzylamine)(N-methylimidazole)2]BPh₄

There total 1 articles about trans-[Co(N,N'-bis(pyrrol-2-ylmethylene)-2-aminobenzylamine)(N-methylimidazole)2]BPh₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

1-methyl-1H-imidazole (616-47-7) + N,N'-bis((1H-pyrrol-2-yl)methylene)-2-aminobenzylamine (1309802-60-5) + sodium tetraphenyl borate (143-66-8) + cobalt(II) diacetate tetrahydrate (6147-53-1) → trans-[Co(N,N'-bis(pyrrol-2-ylmethylene)-2-aminobenzylamine)(N-methylimidazole)2]BPh4 (1309802-53-6)

Guidance literature:

In methanol; to soln. Co(OAc)2*4H2O in MeOH Schiff base ligand in MeOH was added, N-methylimidazole was added dropwise over 45 min, stirred at room temp. for15 min; soln. was filtered, NaBPh4 in MeOH was added, soln. was left at room temp. for a few hours, ppt. was filtered, washed with cold MeOH and dried in vacuo; elem. anal.;

DOI:10.1016/j.poly.2011.03.041

upstream raw materials:

1-methyl-1H-imidazole

N,N'-bis((1H-pyrrol-2-yl)methylene)-2-aminobenzylamine

sodium tetraphenyl borate

cobalt(II) diacetate tetrahydrate

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