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Technology Process of CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4(1+)*I(1-)=(CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4)I

CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4(1+)*I(1-)=(CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4)I

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  • Chemical Name:CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4(1+)*I(1-)=(CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4)I
  • CAS No.:1173700-02-1
  • Molecular Formula:C22H29N2*I
  • Molecular Weight:448.39
  • Hs Code.:
CH<sub>3</sub>NC<sub>3</sub>H<sub>3</sub>NC(CH<sub>3</sub>)(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>C<sub>5</sub>H(CH<sub>3</sub>)4<sup>(1+)</sup>*I<sup>(1-)</sup>=(CH<sub>3</sub>NC<sub>3</sub>H<sub>3</sub>NC(CH<sub>3</sub>)(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>C<sub>5</sub>H(CH<sub>3</sub>)4)I

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Chemical Property of CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4(1+)*I(1-)=(CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4)I
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Technology Process of CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4(1+)*I(1-)=(CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4)I

There total 1 articles about CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4(1+)*I(1-)=(CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4)I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C<sub>21</sub>H<sub>26</sub>N<sub>2</sub>
1192225-30-1

C21H26N2

methyl iodide
74-88-4

methyl iodide

CH<sub>3</sub>NC<sub>3</sub>H<sub>3</sub>NC(CH<sub>3</sub>)(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>C<sub>5</sub>H(CH<sub>3</sub>)4<sup>(1+)</sup>*I<sup>(1-)</sup>=(CH<sub>3</sub>NC<sub>3</sub>H<sub>3</sub>NC(CH<sub>3</sub>)(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>C<sub>5</sub>H(CH<sub>3</sub>)4)I
1173700-02-1

CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4(1+)*I(1-)=(CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4)I

Guidance literature:
In methanol; at 20 ℃; for 12h;
DOI:10.1039/b901195a

Reference yield: 51.0%

chloro(1,5-cyclooctadiene)rhodium(I) dimer

chloro(1,5-cyclooctadiene)rhodium(I) dimer

CH<sub>3</sub>NC<sub>3</sub>H<sub>3</sub>NC(CH<sub>3</sub>)(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>C<sub>5</sub>H(CH<sub>3</sub>)4<sup>(1+)</sup>*I<sup>(1-)</sup>=(CH<sub>3</sub>NC<sub>3</sub>H<sub>3</sub>NC(CH<sub>3</sub>)(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>C<sub>5</sub>H(CH<sub>3</sub>)4)I
1173700-02-1

CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4(1+)*I(1-)=(CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4)I

potassium iodide
7681-11-0

potassium iodide

[η5-tetramethylcyclopentadienyl-CH2C(Ph)(Me)NC3H2NMe]RhI2

[η5-tetramethylcyclopentadienyl-CH2C(Ph)(Me)NC3H2NMe]RhI2

Guidance literature:
With Ag2O; acetic acid; In methanol; Ag2O and imidazolium salt refluxed in 1,2-dichloroethane for 1 h; Rh complex added; refluxed for 30 min; glacial acetic acid added; refluxed overnight; filtered (Celite); filtrate evapd. to dryness; KI and MeOH added; refluxed overnight; cooled; solvent removed under vac.; purified by flash chromy. (CH2Cl2-acetone); elem. anal.;
DOI:10.1039/b901195a

Reference yield: 24.0%

bis(1,5-cyclooctadiene)diiridium(I) dichloride
12112-67-3

bis(1,5-cyclooctadiene)diiridium(I) dichloride

CH<sub>3</sub>NC<sub>3</sub>H<sub>3</sub>NC(CH<sub>3</sub>)(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>C<sub>5</sub>H(CH<sub>3</sub>)4<sup>(1+)</sup>*I<sup>(1-)</sup>=(CH<sub>3</sub>NC<sub>3</sub>H<sub>3</sub>NC(CH<sub>3</sub>)(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>C<sub>5</sub>H(CH<sub>3</sub>)4)I
1173700-02-1

CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4(1+)*I(1-)=(CH3NC3H3NC(CH3)(C6H5)CH2C5H(CH3)4)I

potassium iodide
7681-11-0

potassium iodide

[η5-tetramethylcyclopentadienyl-CH2C(Ph)(Me)NC3H2NMe]IrI2

[η5-tetramethylcyclopentadienyl-CH2C(Ph)(Me)NC3H2NMe]IrI2

Guidance literature:
With Ag2O; acetic acid; In methanol; Ag2O and imidazolium salt refluxed in 1,2-dichloroethane for 1 h; Ir complex added; refluxed for 30 min; glacial acetic acid added; refluxed overnight; filtered (Celite); filtrate evapd. to dryness; KI and MeOH added; refluxed for 16 h; cooled; solvent removed under vac.; purified by flash chromy. (CH2Cl2-acetone);
DOI:10.1039/b901195a
upstream raw materials:

C21H26N2

methyl iodide

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