tert-butyl 2,2′-(2-(2-((((1-(2-tert-butoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

Base Information

Chemical Name:tert-butyl 2,2′-(2-(2-((((1-(2-tert-butoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate
CAS No.:1417889-99-6
Molecular Formula:C₃₆H₅₃N₇O₉S
Molecular Weight:759.924
Hs Code.:

tert-butyl 2,2′-(2-(2-((((1-(2-tert-butoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

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Chemical Property of tert-butyl 2,2′-(2-(2-((((1-(2-tert-butoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

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Technology Process of tert-butyl 2,2′-(2-(2-((((1-(2-tert-butoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

There total 4 articles about tert-butyl 2,2′-(2-(2-((((1-(2-tert-butoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1226869-60-8
tert-butyl 2-(2-formyl-1H-imidazol-1-yl)acetate

: 1446011-66-0
tert-butyl 2,2′-(2-(2-((4-sulfamoylphenethylamino)-methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

: 1417889-99-6
tert-butyl 2,2′-(2-(2-((((1-(2-tert-butoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm3015348

Reference yield:

: 35303-76-5
4-(2-aminoethyl)benzenesulfonamide

: 1417889-99-6
tert-butyl 2,2′-(2-(2-((((1-(2-tert-butoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 1,2-dichloro-ethane / 0.5 h / 75 °C / Inert atmosphere

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere

3: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere

With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane;
DOI:10.1021/jm3015348

Reference yield:

: 1228647-94-6
tert-butyl 2,2′-(2-(2-formyl-1H-imidazol-1-yl)-acetylazanediyl)diacetate

: 1417889-99-6
tert-butyl 2,2′-(2-(2-((((1-(2-tert-butoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 1,2-dichloro-ethane / 0.5 h / 75 °C / Inert atmosphere

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere

3: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere

With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane;
DOI:10.1021/jm3015348