tert-butyl 2,2′-(2-(2-((4-sulfamoylphenethylamino)-methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

Base Information

• Chemical Name: tert-butyl 2,2′-(2-(2-((4-sulfamoylphenethylamino)-methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate
• CAS No.: 1446011-66-0
• Molecular Formula: C₂₆H₃₉N₅O₇S
• Molecular Weight: 565.691

Synonyms:tert-butyl 2,2′-(2-(2-((4-sulfamoylphenethylamino)-methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

Chemical Property of tert-butyl 2,2′-(2-(2-((4-sulfamoylphenethylamino)-methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of tert-butyl 2,2′-(2-(2-((4-sulfamoylphenethylamino)-methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

There total 4 articles about tert-butyl 2,2′-(2-(2-((4-sulfamoylphenethylamino)-methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

tert-butyl 2,2′-(2-(2-formyl-1H-imidazol-1-yl)-acetylazanediyl)diacetate (1228647-94-6) + 4-(2-aminoethyl)benzenesulfonamide (35303-76-5) → tert-butyl 2,2′-(2-(2-((4-sulfamoylphenethylamino)-methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate (1446011-66-0)

Guidance literature:

tert-butyl 2,2′-(2-(2-formyl-1H-imidazol-1-yl)-acetylazanediyl)diacetate; 4-(2-aminoethyl)benzenesulfonamide; With acetic acid; In 1,2-dichloro-ethane; at 75 ℃; for 0.5h; Inert atmosphere;

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

C26H37N5O7S → tert-butyl 2,2′-(2-(2-((4-sulfamoylphenethylamino)-methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate (1446011-66-0)

Guidance literature:

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/jm3015348

Reference yield:

4-(2-aminoethyl)benzenesulfonamide (35303-76-5) → tert-butyl 2,2′-(2-(2-((4-sulfamoylphenethylamino)-methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate (1446011-66-0)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / 1,2-dichloro-ethane / 0.5 h / 75 °C / Inert atmosphere

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere

With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane;

DOI:10.1021/jm3015348

upstream raw materials:

4-(2-aminoethyl)benzenesulfonamide

tert-butyl 2,2′-(2-(2-formyl-1H-imidazol-1-yl)-acetylazanediyl)diacetate

Downstream raw materials:

tert-butyl 2,2′-(2-(2-((((1-(2-tert-butoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

di-tert-butyl 4-(2-(2-((((1-(2-(bis(2-(tert-butoxy)-2-oxoethyl)-amino)-2-oxoethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)acetamido)-4-(3-(tert-butoxy)-3-oxopropyl)heptanedioate

2,2′-(2-(2-((((1-(carboxymethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)-acetylazanediyl)diacetic acid rhenium tricarbonyl complex

C₃₄H₄₄N₈O₁₄S

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