2,2′-(2-(2-((((1-(carboxymethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)-acetylazanediyl)diacetic acid rhenium tricarbonyl complex

Base Information

Chemical Name:2,2′-(2-(2-((((1-(carboxymethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)-acetylazanediyl)diacetic acid rhenium tricarbonyl complex
CAS No.:1417996-82-7
Molecular Formula:C₂₇H₂₉N₇O₁₂ReS
Molecular Weight:861.84
Hs Code.:

2,2′-(2-(2-((((1-(carboxymethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)-acetylazanediyl)diacetic acid rhenium tricarbonyl complex

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Chemical Property of 2,2′-(2-(2-((((1-(carboxymethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)-acetylazanediyl)diacetic acid rhenium tricarbonyl complex

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Technology Process of 2,2′-(2-(2-((((1-(carboxymethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)-acetylazanediyl)diacetic acid rhenium tricarbonyl complex

There total 6 articles about 2,2′-(2-(2-((((1-(carboxymethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)-acetylazanediyl)diacetic acid rhenium tricarbonyl complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₅₃N₇O₁₂ReS⁽¹⁺⁾

: 1417996-82-7
2,2′-(2-(2-((((1-(carboxymethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)-acetylazanediyl)diacetic acid rhenium tricarbonyl complex

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jm3015348

Reference yield:

: 1417889-99-6
tert-butyl 2,2′-(2-(2-((((1-(2-tert-butoxy-2-oxoethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)acetylazanediyl)diacetate

: 1417996-82-7
2,2′-(2-(2-((((1-(carboxymethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)-acetylazanediyl)diacetic acid rhenium tricarbonyl complex

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 4 h / 90 °C / Sealed tube; Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

With trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1021/jm3015348

Reference yield:

: 35303-76-5
4-(2-aminoethyl)benzenesulfonamide

: 1417996-82-7
2,2′-(2-(2-((((1-(carboxymethyl)-1H-imidazol-2-yl)methyl)(4-sulfamoylphenethyl)amino)methyl)-1H-imidazol-1-yl)-acetylazanediyl)diacetic acid rhenium tricarbonyl complex

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / 1,2-dichloro-ethane / 0.5 h / 75 °C / Inert atmosphere

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere

3: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere

4: methanol / 4 h / 90 °C / Sealed tube; Inert atmosphere

5: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

With sodium tris(acetoxy)borohydride; acetic acid; trifluoroacetic acid; In methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jm3015348