4-Benzolazo-phenylacetaldehyd

Base Information

• Chemical Name: 4-Benzolazo-phenylacetaldehyd
• CAS No.: 3516-80-1
• Molecular Formula: C₁₄H₁₂N₂O
• Molecular Weight: 224.262
• Mol file: 3516-80-1.mol

Synonyms:

Chemical Property of 4-Benzolazo-phenylacetaldehyd

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-Benzolazo-phenylacetaldehyd

There total 4 articles about 4-Benzolazo-phenylacetaldehyd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4'-aminophenyl)ethyl alcohol (104-10-9) → 4-Benzolazo-phenylacetaldehyd (3516-80-1)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / dichloromethane

2: Dess-Martin periodane / dichloromethane / 3 h

With Dess-Martin periodane; acetic acid; In dichloromethane;

DOI:10.1002/anie.201309633

Reference yield:

Nitrosobenzene (586-96-9) → 4-Benzolazo-phenylacetaldehyd (3516-80-1)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / dichloromethane

2: Dess-Martin periodane / dichloromethane / 3 h

With Dess-Martin periodane; acetic acid; In dichloromethane;

DOI:10.1002/anie.201309633

Reference yield:

4-[(phenyldiazenyl)phenyl]ethanol → 4-Benzolazo-phenylacetaldehyd (3516-80-1)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; for 3h;

DOI:10.1002/anie.201309633

upstream raw materials:

<4-Benzolazo-phenacetyl>-malonsaeure-diethylester

2-(4'-aminophenyl)ethyl alcohol

Nitrosobenzene

Downstream raw materials:

C₂₈H₃₂N₄O