[(cyclopentadienyl)Cr(III)Me(2,6-(Me₂CH)2C₆H₃NC(Me)CH(Me)NC₆H₄Me)]

Base Information

Chemical Name:[(cyclopentadienyl)Cr(III)Me(2,6-(Me₂CH)2C₆H₃NC(Me)CH(Me)NC₆H₄Me)]
CAS No.:1262528-66-4
Molecular Formula:C₃₀H₃₉CrN₂
Molecular Weight:479.649
Hs Code.:

[(cyclopentadienyl)Cr(III)Me(2,6-(Me<sub>2</sub>CH)2C<sub>6</sub>H<sub>3</sub>NC(Me)CH(Me)NC<sub>6</sub>H<sub>4</sub>Me)]

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Chemical Property of [(cyclopentadienyl)Cr(III)Me(2,6-(Me₂CH)2C₆H₃NC(Me)CH(Me)NC₆H₄Me)]

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Technology Process of [(cyclopentadienyl)Cr(III)Me(2,6-(Me₂CH)2C₆H₃NC(Me)CH(Me)NC₆H₄Me)]

There total 3 articles about [(cyclopentadienyl)Cr(III)Me(2,6-(Me₂CH)2C₆H₃NC(Me)CH(Me)NC₆H₄Me)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1262528-60-8
CpCr[DppNC(Me)CHC(Me)NTol]

: 74-88-4
methyl iodide

: 1262528-66-4
[(cyclopentadienyl)Cr(III)Me(2,6-(Me₂CH)2C₆H₃NC(Me)CH(Me)NC₆H₄Me)]

Guidance literature:: With SmI₂; In tetrahydrofuran; (N2); addn. of soln. of methyl iodide in MTBE to THF soln. of chromium compd., addn. of samarium compd. in THF, stirring for 3 h; evapn., extn. (hexanes), filtration through celite, keeping at -30°C for several ds, isolation of ppt., elem. anal.;
DOI:10.1021/om100961f

Reference yield: 26.0%

: 917-64-6
methyl magnesium iodide

: 1262528-60-8
CpCr[DppNC(Me)CHC(Me)NTol]

: 74-88-4
methyl iodide

: 1262528-66-4
[(cyclopentadienyl)Cr(III)Me(2,6-(Me₂CH)2C₆H₃NC(Me)CH(Me)NC₆H₄Me)]

Guidance literature:: In diethyl ether; (N2); addn. of soln. of methyl iodide in MTBE to ethereal soln. of chromim compd., stirring for 1 h, addn. of methylmagnesium iodide in ether, stirring overnight; addn. of dioxane, stirring for 2 h, evapn., extn. (hexanes), filtration through celite, evapn., extn. (hexanes), filtration through celite, keeping at -30°C for several ds, isolation of ppt., elem. anal.;
DOI:10.1021/om100961f

Reference yield:

: 1262528-60-8
CpCr[DppNC(Me)CHC(Me)NTol]

: 74-88-4
methyl iodide

: 1262528-66-4
[(cyclopentadienyl)Cr(III)Me(2,6-(Me₂CH)2C₆H₃NC(Me)CH(Me)NC₆H₄Me)]

: 1262528-62-0
[(cyclopentadienyl)Cr(III)I(2,6-(Me₂CH)2C₆H₃NC(Me)CH(Me)NC₆H₄Me)]

Guidance literature:: In pentane; (N2); addn. of soln. of methyl iodide in methyl tert-butyl ether into pentane soln. of chromium compd.; UV monitoring; Kinetics;
DOI:10.1021/om100961f