C₃₂H₅₄N₂O₅

Base Information

• Chemical Name: C₃₂H₅₄N₂O₅
• CAS No.: 1312928-09-8
• Molecular Formula: C₃₂H₅₄N₂O₅
• Molecular Weight: 546.791
• Mol file: 1312928-09-8.mol

Synonyms:

Chemical Property of C₃₂H₅₄N₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₂H₅₄N₂O₅

There total 4 articles about C₃₂H₅₄N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C24H30N2O6 (1312927-86-8) → C32H54N2O5 (1312928-09-8)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; palladium 10% on activated carbon; hydrogen / methanol

2: sodium hydrogencarbonate / dichloromethane; water / 4 h

With pyridine; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; In methanol; dichloromethane; water;

DOI:10.1021/jm1016126

Reference yield:

C19H21NO5 (1312927-85-7) → C32H54N2O5 (1312928-09-8)

Guidance literature:

Multi-step reaction with 3 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: pyridine; palladium 10% on activated carbon; hydrogen / methanol

3: sodium hydrogencarbonate / dichloromethane; water / 4 h

With pyridine; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In methanol; dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1021/jm1016126

Reference yield:

β-amino-α-methyl propionic acid methyl ester (14678-48-9) → C32H54N2O5 (1312928-09-8)

Guidance literature:

Multi-step reaction with 3 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: pyridine; palladium 10% on activated carbon; hydrogen / methanol

3: sodium hydrogencarbonate / dichloromethane; water / 4 h

With pyridine; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In methanol; dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1021/jm1016126

upstream raw materials:

C₁₉H₂₁NO₅

C₂₄H₃₀N₂O₆

C₁₆H₂₄N₂O₄

n-hexadecanoyl chloride

Downstream raw materials:

C₃₁H₅₂N₂O₅

C₃₄H₅₇N₃O₆

C₃₃H₅₅N₃O₆