Technology Process of C22H20N2O6S2
There total 5 articles about C22H20N2O6S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hexamethyldisilazane;
In
tetrahydrofuran;
at 0 ℃;
for 0.0833333h;
Inert atmosphere;
DOI:10.1002/anie.201105611
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hypochlorite; sulfuric acid / water / 0.25 h / 0 °C
2: pyridine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
3: potassium carbonate / acetonitrile / 20 °C / Inert atmosphere
4: palladium diacetate; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate / 1,1-dichloroethane / 18 h / 110 °C / Inert atmosphere
5: lithium hexamethyldisilazane / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere
With
pyridine; sodium hypochlorite; sulfuric acid; palladium diacetate; potassium carbonate; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate; lithium hexamethyldisilazane;
In
tetrahydrofuran; 1,1-dichloroethane; water; acetonitrile;
4: Fujiwara-Moritani reaction;
DOI:10.1002/anie.201105611
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
2: potassium carbonate / acetonitrile / 20 °C / Inert atmosphere
3: palladium diacetate; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate / 1,1-dichloroethane / 18 h / 110 °C / Inert atmosphere
4: lithium hexamethyldisilazane / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere
With
pyridine; palladium diacetate; potassium carbonate; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate; lithium hexamethyldisilazane;
In
tetrahydrofuran; 1,1-dichloroethane; acetonitrile;
3: Fujiwara-Moritani reaction;
DOI:10.1002/anie.201105611