chloro(bis(2-(di-tert-butylphosphino)ethyl) ether)(η1-dinitrogen)ruthenium tetraphenylborate*(dichloromethane)

Base Information

Chemical Name:chloro(bis(2-(di-tert-butylphosphino)ethyl) ether)(η1-dinitrogen)ruthenium tetraphenylborate*(dichloromethane)
CAS No.:852995-10-9
Molecular Formula:CH₂Cl₂*C₂₀H₄₄ClN₂OP₂Ru*C₂₄H₂₀B
Molecular Weight:931.219
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of chloro(bis(2-(di-tert-butylphosphino)ethyl) ether)(η1-dinitrogen)ruthenium tetraphenylborate*(dichloromethane)

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Technology Process of chloro(bis(2-(di-tert-butylphosphino)ethyl) ether)(η1-dinitrogen)ruthenium tetraphenylborate*(dichloromethane)

There total 1 articles about chloro(bis(2-(di-tert-butylphosphino)ethyl) ether)(η1-dinitrogen)ruthenium tetraphenylborate*(dichloromethane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 852995-05-2
dichloro(bis(2-(di-tert-butylphosphino)ethyl) ether)ruthenium

: 75-09-2
dichloromethane

: 7727-37-9
nitrogen

: 143-66-8
sodium tetraphenyl borate

: 852995-10-9
chloro(bis(2-(di-tert-butylphosphino)ethyl) ether)(η1-dinitrogen)ruthenium tetraphenylborate*(dichloromethane)

Guidance literature:: In dichloromethane; byproducts: NaCl; under N2; CH2Cl2 added to mixt. of Ru complex and NaBPh4 (molar ratio 1:1); stirred for 3 h; kept at -30°C overnight; filtered; vol. of filtrate reduced; hexane added; crystd. at -30°C overnight; filtered; ppt. washed with hexane; elem. anal.;
DOI:10.1021/om050053v