{(dppe)(η-C6H6)ReH2}{BF4}

Base Information

Chemical Name:{(dppe)(η-C6H6)ReH2}{BF4}
CAS No.:142196-05-2
Molecular Formula:BF₄*C₃₂H₃₂P₂Re
Molecular Weight:751.565
Hs Code.:

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Chemical Property of {(dppe)(η-C6H6)ReH2}{BF4}

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Technology Process of {(dppe)(η-C6H6)ReH2}{BF4}

There total 1 articles about {(dppe)(η-C6H6)ReH2}{BF4} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 142196-02-9
{(dppe)(η-C6H6)ReH}

: 142196-05-2
{(dppe)(η-C6H6)ReH2}{BF4}

Guidance literature:: In diethyl ether; HBF4*Et2O was added to a soln. of ((dppe)(C6H6)ReH) in Et2O, colorless microcrystals immediately deposited, these were filtered off;; washed with Et2O, dried under vacuum; elem. anal.;;
DOI:10.1016/0022-328X(92)80072-6

Reference yield: 68.0%

: 142196-05-2
{(dppe)(η-C6H6)ReH2}{BF4}

: {(dppe)(η-C6H7)ReH2}

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; LiAlH4 was added to a soln. of ((dppe)(C6H6)ReH2)(BF4) in Et2O, the mixture was stirred for 1 h, hydrolyzed with a few drops of H2O and filtered, the solvent was evaporated;; residue was extracted with CH2Cl2, after evaporation the yellow product was recrystd. from acetone; elem. anal.;;
DOI:10.1016/0022-328X(92)80072-6