N-phenyl allyldiphenylphosphinimine

Base Information

• Chemical Name: N-phenyl allyldiphenylphosphinimine
• CAS No.: 110655-46-4
• Molecular Formula: C₂₁H₂₀NP
• Molecular Weight: 317.37
• Mol file: 110655-46-4.mol

Synonyms:

Chemical Property of N-phenyl allyldiphenylphosphinimine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-phenyl allyldiphenylphosphinimine

There total 1 articles about N-phenyl allyldiphenylphosphinimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Phenyl azide (622-37-7) + allyldiphenylphosphine (2741-38-0) → N-phenyl allyldiphenylphosphinimine (110655-46-4)

Guidance literature:

In benzene; at 0 ℃;

DOI:10.1016/S0040-4039(00)82865-8

Reference yield:

N-phenyl allyldiphenylphosphinimine (110655-46-4) → 4-Hydroxy-1,1-diphenyl-3-[(E)-phenylimino]-5-vinyl-3H-1λ5-phosphole-2-carboxylic acid methyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 4 h / Ambient temperature

2: 1.) KH, 2.) MeOH / 1.) THF, 50 deg C, 6 h

With methanol; potassium hydride; In tetrahydrofuran;

DOI:10.1039/c39860001574

Reference yield:

N-phenyl allyldiphenylphosphinimine (110655-46-4) + dimethyl acetylenedicarboxylate (762-42-5) → 2-(Allyl-diphenyl-λ5-phosphanylidene)-3-[(Z)-phenylimino]-succinic acid dimethyl ester

Guidance literature:

In tetrahydrofuran; for 4h; Yield given; Ambient temperature;

DOI:10.1039/c39860001574

upstream raw materials:

Phenyl azide

allyldiphenylphosphine

Downstream raw materials:

N-phenyl 1-propenyldiphenylphosphinimine