2-O2S(O)C6H4Me-p>(iPr3P)2>

Base Information

Chemical Name:2-O2S(O)C6H4Me-p>(iPr3P)2>
CAS No.:219970-52-2
Molecular Formula:C₂₅H₄₉O₃P₂RhS
Molecular Weight:594.581
Hs Code.:

<Rh<η<sup>2</sup>-O2S(O)C6H4Me-p>(iPr3P)2>

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Chemical Property of 2-O2S(O)C6H4Me-p>(iPr3P)2>

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Technology Process of 2-O2S(O)C6H4Me-p>(iPr3P)2>

There total 2 articles about 2-O2S(O)C6H4Me-p>(iPr3P)2> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: Rh(η3-C3H5)(P(i-Pr)3)2

: 104-15-4
toluene-4-sulfonic acid

: 219970-52-2
2-O2S(O)C6H4Me-p>(iPr3P)2>

Guidance literature:: In toluene; (argon); stirring (room temp., 1 h); solvent removal (vac.), extn. (acetone), concn. (vac.), filtration, washing (acetone, 0°C), drying; elem. anal.;
DOI:10.1039/a805900d

Reference yield: 72.0%

: 219970-58-8
[Rh₂(O₃SC₆H₄CH₃)2(C₈H₁₄)4]

: 6476-36-4
tris(1-methylethyl)phosphine

: 219970-52-2
2-O2S(O)C6H4Me-p>(iPr3P)2>

Guidance literature:: In diethyl ether; (argon); stirring (-78°C, 5 min); solvent removal (vac.), dissoln. (pentane), storage (-78°C, 12 h);
DOI:10.1039/a805900d

Reference yield: 95.0%

: 219970-52-2
2-O2S(O)C6H4Me-p>(iPr3P)2>

: 1333-74-0
hydrogen

: 219970-61-3
[RhH₂(O₃SC₆H₄CH₃)(P(C₃H₇)3)2]

Guidance literature:: In dichloromethane; (argon); passing a H2 stream for ca. 5 s through the soln. of the Rh complex in CH2Cl2, stirring (room temp., 15 min); solvent removal (vac.), washing (pentane, -78°C, drying (vac., < 5 min); elem. anal.;
DOI:10.1039/a805900d