1-tricarbonylchromium⁽⁰⁾phenyl-1.1.2.2-tetraphenylethane

Base Information

Chemical Name:1-tricarbonylchromium⁽⁰⁾phenyl-1.1.2.2-tetraphenylethane
CAS No.:121699-89-6
Molecular Formula:C₃₅H₂₆CrO₃
Molecular Weight:546.586
Hs Code.:

1-tricarbonylchromium<sup>(0)</sup>phenyl-1.1.2.2-tetraphenylethane

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Chemical Property of 1-tricarbonylchromium⁽⁰⁾phenyl-1.1.2.2-tetraphenylethane

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Technology Process of 1-tricarbonylchromium⁽⁰⁾phenyl-1.1.2.2-tetraphenylethane

There total 2 articles about 1-tricarbonylchromium⁽⁰⁾phenyl-1.1.2.2-tetraphenylethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 12147-93-2
diphenylmethylchloride tricarbonylchromium⁽⁰⁾

: 596-43-0
bromo-triphenyl-methane

: 121699-87-4,121699-89-6
2-tricarbonylchromium⁽⁰⁾phenyl-1.1.1.2-tetraphenylethane

Guidance literature:: With Mg; In benzene; Triphenylmethylbromide and Mg in benzene/ether formed Grignard reagent, this treated with benzhydryl chloride tricarbonylchromium(0) and stirred overnight.; Extn. with ether, recrystn. from benzene/cyclopentane; elem. anal.;
DOI:10.1016/0022-328X(88)80341-3

Reference yield: 65.7%

: 73016-86-1
(η6-triphenylmethane)chromium tricarbonyl

: 776-74-9
Bromodiphenylmethane

: 121699-89-6,121699-87-4
1-tricarbonylchromium⁽⁰⁾phenyl-1.1.2.2-tetraphenylethane

Guidance literature:: With n-C₄H₉OK; In tetrahydrofuran; To soln. of η-6-chromium tricarbonyl complex of triphenylmethane, n-C4H9OK in THF added Ph2CHBr and stirred overnight at 25°C.; Extn. with ether, recrystn. from benzene/petroleum ether; elem. anal.;
DOI:10.1016/0022-328X(88)80341-3

Reference yield: 78.0%

: 121699-87-4,121699-89-6
2-tricarbonylchromium⁽⁰⁾phenyl-1.1.1.2-tetraphenylethane

: 19112-42-6
pentaphenylethane

Guidance literature:: With ceric ammonium nitrate; In diethyl ether; acetonitrile; (C6H5)3CCH(C6H5)(C6H5)Cr(CO)3 in ether/acetonitrile stirred with 0.2 N soln. of ceric ammonium nitrate until soln. became nearly colourless.;
DOI:10.1016/0022-328X(88)80341-3