C₂₉H₃₅NO₅Si

Base Information

Chemical Name:C₂₉H₃₅NO₅Si
CAS No.:1562377-37-0
Molecular Formula:C₂₉H₃₅NO₅Si
Molecular Weight:505.686
Hs Code.:

C<sub>29</sub>H<sub>35</sub>NO<sub>5</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₅NO₅Si

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Technology Process of C₂₉H₃₅NO₅Si

There total 2 articles about C₂₉H₃₅NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1562377-09-6
C₂₃H₂₅NO₃

: 18162-48-6
tert-butyldimethylsilyl chloride

: 922-67-8
propynoic acid methyl ester

: 1562377-21-2
C₂₉H₃₅NO₅Si

: 1562377-37-0
C₂₉H₃₅NO₅Si

Guidance literature:: C₂₃H₂₅NO₃; With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; at -78 ℃; Molecular sieve; Inert atmosphere;

tert-butyldimethylsilyl chloride; In tetrahydrofuran; at -78 - 20 ℃; for 7h; Molecular sieve; Inert atmosphere;

propynoic acid methyl ester; at 150 ℃; Overall yield = 62 %; Overall yield = 94 mg; regioselective reaction; Sealed tube; Inert atmosphere;
DOI:10.1021/ol4034447

Reference yield:

: 889-31-6
5,5-dimethyl-3-benzylamino-2-cyclohexen-1-one

: 1562377-37-0
C₂₉H₃₅NO₅Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C / Molecular sieve; Inert atmosphere

1.2: -78 - 20 °C / Molecular sieve; Inert atmosphere

2.1: n-butyllithium; potassium tert-butylate / tetrahydrofuran / -78 °C / Molecular sieve; Inert atmosphere

2.2: 7 h / -78 - 20 °C / Molecular sieve; Inert atmosphere

2.3: 255 / 150 °C / Sealed tube; Inert atmosphere

With n-butyllithium; potassium tert-butylate; In tetrahydrofuran;
DOI:10.1021/ol4034447