dibenzyldineophyltin

Base Information

Chemical Name:dibenzyldineophyltin
CAS No.:1299472-00-6
Molecular Formula:C₃₄H₄₀Sn
Molecular Weight:567.402
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzyldineophyltin

Chemical Property:

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Technology Process of dibenzyldineophyltin

There total 1 articles about dibenzyldineophyltin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.6%

: 35293-35-7
2-methyl-2-phenyl-1-propylmagnesium chloride

: 3002-01-5
dibenzyltin(IV) dichloride

: 1299472-00-6
dibenzyldineophyltin

Guidance literature:: In diethyl ether; 1.44M Et2O soln. of NeophMgCl (0.072 mmol) dropwise with stirring added to Et2O soln. of (PhCH2)2SnCl2 (0.032 mmol) under N2 at room temp., stirred at room temp. for 12 h, heated at reflux for 2 h; aq. satd. soln. NH4Cl added, organic layer separated, aq. layer extracted with Et2O, combined organic extracts dried over MgSO4, filtered, solvent removed under vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2010.12.033

Reference yield: 88.0%

: 1299472-00-6
dibenzyldineophyltin

: 7726-95-6
bromine

: 131025-88-2
bis(2-methyl-2-phenylpropyl)tin dibromide

Guidance literature:: In tetrachloromethane; CCl4 soln. of Br2 (3 mmol) dropwise with stirring added to CCl4 soln. of(PhCH2)2SnNeoph2 (2.91 mmol) under N2 in dark; solvent with PhCH2Br removed under vac., chromd. (silica gel 60; n-hexane/Et2O (96:4)); elem. anal.;
DOI:10.1016/j.jorganchem.2010.12.033

Reference yield:

: 1299472-00-6
dibenzyldineophyltin

: 1299472-01-7
di[(Z)-2-phenylvinyl]dineophyltin

Guidance literature:: Multi-step reaction with 3 steps

1: tetrachloromethane

2: diethyl ether

3: azobisisobutyronitrile / neat (no solvent)

With azobisisobutyronitrile; In tetrachloromethane; diethyl ether;
DOI:10.1016/j.jorganchem.2010.12.033