C₁₂H₁₄INO₂

Base Information

Chemical Name:C₁₂H₁₄INO₂
CAS No.:1350809-94-7
Molecular Formula:C₁₂H₁₄INO₂
Molecular Weight:331.153
Hs Code.:

C<sub>12</sub>H<sub>14</sub>INO<sub>2</sub>

Synonyms:

Suppliers and Price of C₁₂H₁₄INO₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₄INO₂

Chemical Property:

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Technology Process of C₁₂H₁₄INO₂

There total 4 articles about C₁₂H₁₄INO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₂₁IO₃

: 1350809-94-7
C₁₂H₁₄INO₂

Guidance literature:: Multi-step reaction with 2 steps

1: water; toluene-4-sulfonic acid / acetone / 80 °C

2: ethanol / 6 h / 20 °C

With water; toluene-4-sulfonic acid; In ethanol; acetone;
DOI:10.1039/c1cc15257b

Reference yield:

: 70396-10-0
(Z)-3-iodo-2-phenyl-prop-2-en-1-ol

: 1350809-94-7
C₁₂H₁₄INO₂

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

2: water; toluene-4-sulfonic acid / acetone / 80 °C

3: ethanol / 6 h / 20 °C

With water; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; acetone;
DOI:10.1039/c1cc15257b

Reference yield:

: 100-58-3
phenylmagnesium bromide

: 1350809-94-7
C₁₂H₁₄INO₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) iodide / diethyl ether / 18 h / -78 - 20 °C / Inert atmosphere

1.2: 1 h / -78 - 20 °C

1.3: 0 °C / Saturated gas

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

3.1: water; toluene-4-sulfonic acid / acetone / 80 °C

4.1: ethanol / 6 h / 20 °C

With copper(l) iodide; water; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; ethanol; acetone;
DOI:10.1039/c1cc15257b