tris(2,6-dimethylphenyl)tin(IV) hydroxide

Base Information

Chemical Name:tris(2,6-dimethylphenyl)tin(IV) hydroxide
CAS No.:1259532-87-0
Molecular Formula:C₂₄H₂₈OSn
Molecular Weight:451.196
Hs Code.:

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Chemical Property of tris(2,6-dimethylphenyl)tin(IV) hydroxide

Chemical Property:

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Technology Process of tris(2,6-dimethylphenyl)tin(IV) hydroxide

There total 4 articles about tris(2,6-dimethylphenyl)tin(IV) hydroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 576-22-7
2-Bromo-m-xylene

: 7646-78-8
tin(IV) chloride

: 1259532-87-0
tris(2,6-dimethylphenyl)tin(IV) hydroxide

Guidance literature:: With Mg; In tetrahydrofuran; benzene; Br compd. was added dropwise to Mg (3.85 equiv.) and THF; refluxed for 19 h; cooled to room temp.; added dropwise to soln. of SnCl4 (1 equiv.) in C6H6 at 0°C; refluxed for 5 h; filtered through Celite; washed (aq. HCl); evapd. (vac.); dissolved in toluene; poured into aq. NaOH; refluxed for 18 h; cooled to room temp.; septd.; aq. layer extd. (Et2O); combined org. phase dried (Na2SO4); evapd. (vac.); crystd. (C6H6); elem. anal.;
DOI:10.1039/c0dt00812e

Reference yield:

: 576-22-7
2-Bromo-m-xylene

: 1259532-87-0
tris(2,6-dimethylphenyl)tin(IV) hydroxide

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium / diethyl ether

2: diethyl ether / 60 h / Inert atmosphere

3: dichloromethane; methanol; water / 20 °C

With magnesium; In methanol; diethyl ether; dichloromethane; water;