3-methyl-5-benzylideneamino-6-benzylidenehydrazinouracil

Base Information

Chemical Name:3-methyl-5-benzylideneamino-6-benzylidenehydrazinouracil
CAS No.:675873-43-5
Molecular Formula:C₁₉H₁₇N₅O₂
Molecular Weight:347.376
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methyl-5-benzylideneamino-6-benzylidenehydrazinouracil

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Technology Process of 3-methyl-5-benzylideneamino-6-benzylidenehydrazinouracil

There total 5 articles about 3-methyl-5-benzylideneamino-6-benzylidenehydrazinouracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 3-methyl-5-amino-6-hydrazinouracil

: 100-52-7
benzaldehyde

: 675873-43-5
3-methyl-5-benzylideneamino-6-benzylidenehydrazinouracil

Guidance literature:: In N,N-dimethyl-formamide; for 0.0833333h; Heating;
DOI:10.1007/BF00486922

Reference yield:

: 2565-47-1
1-methyl-2,4,6-pyrimidinetrione

: 675873-43-5
3-methyl-5-benzylideneamino-6-benzylidenehydrazinouracil

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / water, POCl₃ / Heating

2: 77 percent / conc. H₂SO₄, HNO₃ (d= 1.52) / 15 min, 15 deg C then 1 h, 20 deg C

3: 86 percent / 30percent hydrazine / ethanol / 15 min, 20 deg C then 5 min, reflux

4: 88 percent / Na₂S₂O₄, 10percent NH₄OH / 20 min then 5 min, reflux

5: 96 percent / dimethylformamide / 0.08 h / Heating

With ammonium hydroxide; sodium dithionite; sulfuric acid; water; nitric acid; hydrazine hydrate; trichlorophosphate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1007/BF00486922

Reference yield:

: 3-methyl-5-nitro-6-hydrazinouracil hydrazinium salt

: 675873-43-5
3-methyl-5-benzylideneamino-6-benzylidenehydrazinouracil

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / Na₂S₂O₄, 10percent NH₄OH / 20 min then 5 min, reflux

2: 96 percent / dimethylformamide / 0.08 h / Heating

With ammonium hydroxide; sodium dithionite; In N,N-dimethyl-formamide;
DOI:10.1007/BF00486922