C₈⁽¹⁴⁾CH₁₀BrNO₂

Base Information

Chemical Name:C₈⁽¹⁴⁾CH₁₀BrNO₂
CAS No.:1350811-66-3
Molecular Formula:C₉H₁₀BrNO₂
Molecular Weight:246.077
Hs Code.:

C<sub>8</sub><sup>(14)</sup>CH<sub>10</sub>BrNO<sub>2</sub>

Synonyms:

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Chemical Property of C₈⁽¹⁴⁾CH₁₀BrNO₂

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Technology Process of C₈⁽¹⁴⁾CH₁₀BrNO₂

There total 2 articles about C₈⁽¹⁴⁾CH₁₀BrNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆⁽¹⁴⁾CH₄BrClO

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1350811-66-3
C₈⁽¹⁴⁾CH₁₀BrNO₂

Guidance literature:: With pyridine; In dichloromethane; at 23 ℃; Inert atmosphere; Cooling;
DOI:10.1002/jlcr.1879

Reference yield:

: 1192546-40-9
4-bromobenzoic acid[⁽¹⁴⁾C-carboxyl]

: 1350811-66-3
C₈⁽¹⁴⁾CH₁₀BrNO₂

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / toluene / 1 h / 23 °C / Inert atmosphere

2: pyridine / dichloromethane / 23 °C / Inert atmosphere; Cooling

With pyridine; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; toluene;
DOI:10.1002/jlcr.1879

Reference yield:

: 1350811-66-3
C₈⁽¹⁴⁾CH₁₀BrNO₂

: C₂₈⁽¹⁴⁾CH₃₂F₂N₅O₅PS

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrahydrofuran / 18 h / 23 °C / Inert atmosphere; Cooling

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 18 h / Inert atmosphere; Heating

3.1: aluminum (III) chloride; bromine / ethyl acetate / 0.5 h / 5 - 23 °C / Inert atmosphere

4.1: methanol / 1.5 h / Reflux; Inert atmosphere

5.1: iodine; sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 17 °C / Inert atmosphere

5.2: 23 °C / Inert atmosphere

With aluminum (III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; iodine; sodium hydride; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/jlcr.1879