ethyl 2-amino-4-nitrobenzoate

Base Information

• Chemical Name: ethyl 2-amino-4-nitrobenzoate
• CAS No.: 87840-67-3
• Molecular Formula: C₁₈H₂₄N₂O₉
• Molecular Weight: 412.397

Synonyms:

Chemical Property of ethyl 2-amino-4-nitrobenzoate

Chemical Property:

Purity/Quality:

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Technology Process of ethyl 2-amino-4-nitrobenzoate

There total 3 articles about ethyl 2-amino-4-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

ethanol (64-17-5) + diethyl 2,4-dinitrobenzylidenemalonate (87840-68-4) → ethyl 2-amino-4-nitrobenzoate (87840-67-3)

Guidance literature:

With diethylamine; for 24h; Mechanism; Ambient temperature; other amines;

DOI:10.1055/s-1983-30462

Reference yield: 42.0%

ethanol (64-17-5) + diethyl 2,4-dinitrobenzylidenemalonate (87840-68-4) → ethyl 2-amino-4-nitrobenzoate (87840-67-3) + 2-[(diethoxycarbonyl)(ethylthio)-methylamino]-4-nitro-benzoic acid ethyl ester (128609-46-1)

Guidance literature:

With sodium; ethanethiol; Ambient temperature;

Reference yield: 32.0%

ethanol (64-17-5) + diethyl 2,4-dinitrobenzylidenemalonate (87840-68-4) + ethanethiol (75-08-1) → ethyl 2-amino-4-nitrobenzoate (87840-67-3) + 2-[(diethoxycarbonyl)(ethylthio)-methylamino]-4-nitro-benzoic acid ethyl ester (128609-46-1)

Guidance literature:

With sodium; Ambient temperature;

upstream raw materials:

ethanol

diethyl 2,4-dinitrobenzylidenemalonate

ethanethiol

Downstream raw materials:

ethyl 2-amino-4-nitrobenzoate

ethyl 2-amino-4-nitrobenzoate

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