cis-2-methyl-3-phenyl-2,3-dihydrobenzofuran

Base Information

Chemical Name:cis-2-methyl-3-phenyl-2,3-dihydrobenzofuran
CAS No.:38281-39-9
Molecular Formula:C₁₅H₁₄O
Molecular Weight:210.276
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-2-methyl-3-phenyl-2,3-dihydrobenzofuran

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of cis-2-methyl-3-phenyl-2,3-dihydrobenzofuran

There total 16 articles about cis-2-methyl-3-phenyl-2,3-dihydrobenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38276-75-4
2-(1-phenylallyl)phenol

: 38281-39-9,38281-40-2,51677-43-1
trans-2-Methyl-3-phenyldihydrobenzofuran

: 38281-39-9,38281-40-2,51677-43-1
cis-2-Methyl-3-phenyldihydrobenzofuran

: C₁₅H₁₄O

: C₁₅H₁₄O

Guidance literature:: With titanium(IV) 2-ethylhexoxide; water; C₅₄H₆₈N₂O₁₀S₄; In cyclohexane; at 75 ℃; for 48h; Overall yield = 44 percent; enantioselective reaction; Inert atmosphere;
DOI:10.1021/acscatal.1c01146

Reference yield:

: 38276-75-4
2-(1-phenylallyl)phenol

: 38281-39-9,38281-40-2,51677-43-1
trans-2-Methyl-3-phenyldihydrobenzofuran

: 38281-39-9,38281-40-2,51677-43-1
cis-2-Methyl-3-phenyldihydrobenzofuran

: C₁₅H₁₄O

: C₁₅H₁₄O

Guidance literature:: With titanium(IV) 2-ethylhexoxide; water; C₅₄H₆₈N₂O₁₀S₄; In cyclohexane; at 75 ℃; for 48h; Overall yield = 44 percent; enantioselective reaction; Inert atmosphere;
DOI:10.1021/acscatal.1c01146

Reference yield:

: 117-99-7
2-Hydroxybenzophenone

: 38281-39-9,38281-40-2,51677-43-1
trans-2-methyl-3-phenyl-2,3-dihydrobenzofuran

Guidance literature:: Multi-step reaction with 4 steps

1: 92.5 percent / NaOH / dimethylsulfoxide / 40 °C

2: 90.8 percent / hydrazine hydrate / ethanol / Heating

3: Na₂SO₄, yellow HgO, sat. ethanol. KOH / diethyl ether / 10 h / Ambient temperature

4: -196 °C / Irradiation

With potassium hydroxide; sodium hydroxide; hydrazine hydrate; sodium sulfate; mercury(II) oxide; In diethyl ether; ethanol; dimethyl sulfoxide;