OsCl(NO)(CH₂SO)(P(C₆H₅)3)2

Base Information

• Chemical Name: OsCl(NO)(CH₂SO)(P(C₆H₅)3)2
• CAS No.: 109748-85-8
• Molecular Formula: C₃₇H₃₂ClNO₂OsP₂S
• Molecular Weight: 842.333
• Mol file: 109748-85-8.mol

Synonyms:

Chemical Property of OsCl(NO)(CH₂SO)(P(C₆H₅)3)2

Chemical Property:

Purity/Quality:

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Technology Process of OsCl(NO)(CH₂SO)(P(C₆H₅)3)2

There total 1 articles about OsCl(NO)(CH₂SO)(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

OsCl(NO)(SCH2)(P(C6H5)3)2*0.5CH2Cl2 + 3-chloro-benzenecarboperoxoic acid (937-14-4) → OsCl(NO)(CH2SO)(P(C6H5)3)2 (109748-85-8)

Guidance literature:

In dichloromethane; ClC6H4C(O)OOH added under stirring to a soln. of the Os complex (-78°C), warmed up (room temp.); solvent removed, chromatographed (CH2Cl2), crystn. (CH2Cl2/EtOH);

DOI:10.1016/S0022-328X(00)99597-4

upstream raw materials:

3-chloro-benzenecarboperoxoic acid