C₂₀H₂₂Cl₃NO₇

Base Information

Chemical Name:C₂₀H₂₂Cl₃NO₇
CAS No.:1421851-09-3
Molecular Formula:C₂₀H₂₂Cl₃NO₇
Molecular Weight:494.756
Hs Code.:

C<sub>20</sub>H<sub>22</sub>Cl<sub>3</sub>NO<sub>7</sub>

Synonyms:

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Chemical Property of C₂₀H₂₂Cl₃NO₇

Chemical Property:

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Technology Process of C₂₀H₂₂Cl₃NO₇

There total 11 articles about C₂₀H₂₂Cl₃NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 352670-32-7
(1S,4S,5R,6S,8S,9S)-9-(benzyloxy)-6-(dimethoxymethyl)-8-hydroxy-8-methyl-3-oxo-5-(2,2,2-trichloroacetamido)-2-oxabicyclo[3.3.1]nonan-4-yl acetate

: 1421851-09-3
C₂₀H₂₂Cl₃NO₇

: 1421851-10-6
C₂₀H₂₂Cl₃NO₇

Guidance literature:: (1S,4S,5R,6S,8S,9S)-9-(benzyloxy)-6-(dimethoxymethyl)-8-hydroxy-8-methyl-3-oxo-5-(2,2,2-trichloroacetamido)-2-oxabicyclo[3.3.1]nonan-4-yl acetate; With potassium cyanide; In ethanol; at 20 ℃; for 1h; Inert atmosphere;

In methanol; at 20 ℃; for 12h;
DOI:10.1021/jo302773f

Reference yield:

: C₁₂H₁₂Cl₃NO₃

: 1421851-09-3
C₂₀H₂₂Cl₃NO₇

: 1421851-10-6
C₂₀H₂₂Cl₃NO₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: CSA / methanol / 1 h / 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C / Inert atmosphere

3.1: disodium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 30 h / 20 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

4.2: 10 h

5.1: ozone / dichloromethane / 1.5 h / -78 °C / Inert atmosphere

5.2: -78 - 20 °C / Inert atmosphere

6.1: ethylmagnesium bromide / tetrahydrofuran / 0.25 h / 20 °C / Cooling with ice; Inert atmosphere

6.2: 1 h / -20 - 20 °C / Inert atmosphere

7.1: pyridine / 12 h / 20 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / toluene; tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere

9.1: sodium hydrogencarbonate; ruthenium trichloride; Oxone / water; tetrachloromethane; acetonitrile

10.1: potassium cyanide / ethanol / 1 h / 20 °C / Inert atmosphere

10.2: CSA / 12 h / 20 °C

With potassium cyanide; ruthenium trichloride; Oxone; disodium hydrogenphosphate; ethylmagnesium bromide; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; ozone; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/jo302773f

Reference yield:

: 271256-59-8
2,2,2-Trichloro-N-[(1R,6S)-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methyl-2-oxo-1-vinyl-cyclohex-3-enyl]-acetamide

: 1421851-09-3
C₂₀H₂₂Cl₃NO₇

: 1421851-10-6
C₂₀H₂₂Cl₃NO₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: periodic acid dihydrate / ethyl acetate / 4 h / 20 °C / Inert atmosphere

2.1: CSA / methanol / 1 h / 20 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C / Inert atmosphere

4.1: disodium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 30 h / 20 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

5.2: 10 h

6.1: ozone / dichloromethane / 1.5 h / -78 °C / Inert atmosphere

6.2: -78 - 20 °C / Inert atmosphere

7.1: ethylmagnesium bromide / tetrahydrofuran / 0.25 h / 20 °C / Cooling with ice; Inert atmosphere

7.2: 1 h / -20 - 20 °C / Inert atmosphere

8.1: pyridine / 12 h / 20 °C / Inert atmosphere

9.1: tetrabutyl ammonium fluoride / toluene; tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere

10.1: sodium hydrogencarbonate; potassium permanganate; sodium periodate / tert-butyl alcohol; water / 0.5 h / 20 °C

11.1: potassium cyanide / ethanol / 1 h / 20 °C / Inert atmosphere

11.2: CSA / 12 h / 20 °C

With potassium cyanide; potassium permanganate; sodium periodate; disodium hydrogenphosphate; periodic acid dihydrate; ethylmagnesium bromide; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; ozone; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1021/jo302773f