((C₆H₅)2PO)2C₁₀H₆

Base Information

• Chemical Name: ((C₆H₅)2PO)2C₁₀H₆
• CAS No.: 1374033-97-2
• Molecular Formula: C₃₄H₂₆O₂P₂
• Molecular Weight: 528.527
• Mol file: 1374033-97-2.mol

Synonyms:

Chemical Property of ((C₆H₅)2PO)2C₁₀H₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ((C₆H₅)2PO)2C₁₀H₆

There total 1 articles about ((C₆H₅)2PO)2C₁₀H₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-dihydroxynaphthalene (132-86-5) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → ((C6H5)2PO)2C10H6 (1374033-97-2)

Guidance literature:

With triethylamine; In toluene; for 24h; Reflux; Inert atmosphere; Schlenk technique;

DOI:10.1002/ejic.202000425

Reference yield: 83.0%

((C6H5)2PO)2C10H6 (1374033-97-2) + nickel dichloride (83864-14-6) → NiCl((C6H5)2PO)2C10H5 (1374033-98-3)

Guidance literature:

In toluene; toluene soln. of phosphinite added dropwise to suspn. of NiCl2 in toluene, refluxed overnight; filtered over silica gel, washed with Et2O, pumped off to dryness; residue extd. with CH2Cl2, solvent removed under vac.; recrystd. from CH2Cl2/hexane; elem. anal.;

DOI:10.1016/j.ica.2011.12.052

Reference yield: 62.0%

((C6H5)2PO)2C10H6 (1374033-97-2) + [RuCl2(1,5-cyclooctadiene)]n + benzaldehyde (100-52-7) → C35H25ClO3P2Ru

Guidance literature:

With triethylamine; In 1,2-dichloro-ethane; for 24h; Reflux; Inert atmosphere; Schlenk technique;

DOI:10.1002/ejic.202000425

upstream raw materials:

1,3-dihydroxynaphthalene

chloro-diphenylphosphine

Downstream raw materials:

NiCl((C₆H₅)2PO)2C₁₀H₅