Phosphoric acid hexadecyl ester (3aR,4S,4aR,7aS,8S,8aR)-8-hydroxy-2,2,6,6-tetramethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxol-4-yl ester phenyl ester

Base Information

Chemical Name:Phosphoric acid hexadecyl ester (3aR,4S,4aR,7aS,8S,8aR)-8-hydroxy-2,2,6,6-tetramethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxol-4-yl ester phenyl ester
CAS No.:161105-02-8
Molecular Formula:C₃₄H₅₇O₉P
Molecular Weight:640.795
Hs Code.:

Phosphoric acid hexadecyl ester (3aR,4S,4aR,7aS,8S,8aR)-8-hydroxy-2,2,6,6-tetramethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxol-4-yl ester phenyl ester

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Chemical Property of Phosphoric acid hexadecyl ester (3aR,4S,4aR,7aS,8S,8aR)-8-hydroxy-2,2,6,6-tetramethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxol-4-yl ester phenyl ester

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Technology Process of Phosphoric acid hexadecyl ester (3aR,4S,4aR,7aS,8S,8aR)-8-hydroxy-2,2,6,6-tetramethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxol-4-yl ester phenyl ester

There total 4 articles about Phosphoric acid hexadecyl ester (3aR,4S,4aR,7aS,8S,8aR)-8-hydroxy-2,2,6,6-tetramethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxol-4-yl ester phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36653-82-4,124-29-8
1-Hexadecanol

: 161105-02-8
Phosphoric acid hexadecyl ester (3aR,4S,4aR,7aS,8S,8aR)-8-hydroxy-2,2,6,6-tetramethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxol-4-yl ester phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / pyridine / hexane / 1 h / Ambient temperature

2: pyridine, Et₃N, MSNT / 2 h

With pyridine; MSNT; triethylamine; In hexane;
DOI:10.1016/0223-5234(94)90146-5

Reference yield:

: 770-12-7
O-phenyl phosphorodichloridate

: 161105-02-8
Phosphoric acid hexadecyl ester (3aR,4S,4aR,7aS,8S,8aR)-8-hydroxy-2,2,6,6-tetramethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxol-4-yl ester phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / pyridine / hexane / 1 h / Ambient temperature

2: pyridine, Et₃N, MSNT / 2 h

With pyridine; MSNT; triethylamine; In hexane;
DOI:10.1016/0223-5234(94)90146-5

Reference yield:

: 51548-88-0,96039-15-5,98974-89-1,128110-25-8
(+/-)-1,2:4,5-di-O-isopropylidene-myo-inositol

: 161105-02-8
Phosphoric acid hexadecyl ester (3aR,4S,4aR,7aS,8S,8aR)-8-hydroxy-2,2,6,6-tetramethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxol-4-yl ester phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: pyridine, Et₃N, MSNT / 2 h

With pyridine; MSNT; triethylamine;
DOI:10.1016/0223-5234(94)90146-5