2,6-Dichloro-4-nitrobenzene-1-sulfonyl chloride

Base Information

Chemical Name:2,6-Dichloro-4-nitrobenzene-1-sulfonyl chloride
CAS No.:74875-17-5
Molecular Formula:C₆H₂Cl₃NO₄S
Molecular Weight:290.511
Hs Code.:2930909899
European Community (EC) Number:828-847-9

Synonyms:2,6-dichloro-4-nitrobenzene-1-sulfonyl chloride;74875-17-5;2,6-dichloro-4-nitrobenzenesulfonyl chloride;AKOS000147739;CS-0248532;FT-0750395;EN300-40129;2,6-dichloro-4-nitrobenzene-1-sulfonylchloride

Suppliers and Price of 2,6-Dichloro-4-nitrobenzene-1-sulfonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,6-DICHLORO-4-NITROBENZENE-1-SULFONYL CHLORIDE 95.00%
5G
$ 1759.28

American Custom Chemicals Corporation
2,6-DICHLORO-4-NITROBENZENE-1-SULFONYL CHLORIDE 95.00%
2.5G
$ 1363.65

American Custom Chemicals Corporation
2,6-DICHLORO-4-NITROBENZENE-1-SULFONYL CHLORIDE 95.00%
1G
$ 925.31

Total 4 raw suppliers

Chemical Property of 2,6-Dichloro-4-nitrobenzene-1-sulfonyl chloride

Chemical Property:

Melting Point:93-94 °C
Boiling Point:389.0±42.0 °C(Predicted)
Density:1.795±0.06 g/cm3(Predicted)
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:288.877012
Heavy Atom Count:15
Complexity:336

Purity/Quality:

99% ^*data from raw suppliers

2,6-DICHLORO-4-NITROBENZENE-1-SULFONYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=C(C=C(C(=C1Cl)S(=O)(=O)Cl)Cl)[N+](=O)[O-]

Technology Process of 2,6-Dichloro-4-nitrobenzene-1-sulfonyl chloride

There total 1 articles about 2,6-Dichloro-4-nitrobenzene-1-sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74875-16-4
bis(2,6-dichloro-4-nitrophenyl) disulfide

: 74875-17-5
2,6-dichloro-4-nitrobenzenesulfonyl chloride

Guidance literature:: With water; chlorine; for 3.5h;
DOI:10.1021/jm00184a005

Reference yield:

: 74875-17-5
2,6-dichloro-4-nitrobenzenesulfonyl chloride

: 74875-24-4
2-<3,5-dichloro-4-(morpholinylsulfonyl)phenyl>-3,5(2H,4H)-dioxo-as-triazine-6-carboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 2.64 g / diethyl ether / 3 h / Heating

2: 73 percent / SnCl₂*2H₂O, conc. aq. HCl / 1.25 h / Heating

3: 1.) 6 N aq. HCl, NaNO₂, 2.) pyridine / 1.) from 0 to 5 deg C, 2.) RT, 16 h

4: NaOAc, AcOH / 7 h / Heating

5: aq. HCl / acetic acid / 1.5 h / Heating

With pyridine; hydrogenchloride; sodium acetate; acetic acid; tin(ll) chloride; sodium nitrite; In diethyl ether; acetic acid;
DOI:10.1021/jm00184a005

Reference yield:

: 74875-17-5
2,6-dichloro-4-nitrobenzenesulfonyl chloride

: 74875-23-3
ethyl N-<<hydrazinylidene>methyl>carbonyl>carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 2.64 g / diethyl ether / 3 h / Heating

2: 73 percent / SnCl₂*2H₂O, conc. aq. HCl / 1.25 h / Heating

3: 1.) 6 N aq. HCl, NaNO₂, 2.) pyridine / 1.) from 0 to 5 deg C, 2.) RT, 16 h

With pyridine; hydrogenchloride; tin(ll) chloride; sodium nitrite; In diethyl ether;
DOI:10.1021/jm00184a005