2-p-Hydroxyphenyl 3-p-azidophenyl propionyl ethylene diamine monoamide

Base Information

• Chemical Name: 2-p-Hydroxyphenyl 3-p-azidophenyl propionyl ethylene diamine monoamide
• CAS No.: 131374-27-1
• Molecular Formula: C₁₇H₁₉N₅O₂
• Molecular Weight: 325.37
• Mol file: 131374-27-1.mol

Synonyms:

Chemical Property of 2-p-Hydroxyphenyl 3-p-azidophenyl propionyl ethylene diamine monoamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-p-Hydroxyphenyl 3-p-azidophenyl propionyl ethylene diamine monoamide

There total 1 articles about 2-p-Hydroxyphenyl 3-p-azidophenyl propionyl ethylene diamine monoamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + ethylenediamine (107-15-3,85404-18-8) → 2-p-Hydroxyphenyl 3-p-azidophenyl propionyl ethylene diamine monoamide (131374-27-1)

Guidance literature:

In benzene; Yield given; ice cooling;

DOI:10.1016/S0040-4039(00)98057-2

Reference yield:

C54H76O17 (94664-01-4) + 2-p-Hydroxyphenyl 3-p-azidophenyl propionyl ethylene diamine monoamide (131374-27-1) → C71H93N5O18

Guidance literature:

With dicyclohexyl-carbodiimide; In pyridine; at 85 ℃; for 2h;

DOI:10.1016/S0040-4039(00)98057-2

Reference yield:

Forskolin hemisuccinic acid + 2-p-Hydroxyphenyl 3-p-azidophenyl propionyl ethylene diamine monoamide (131374-27-1) → N-{2-[3-(4-Azido-phenyl)-2-(4-hydroxy-phenyl)-propionylamino]-ethyl}-succinamic acid 6,10,10b-trihydroxy-3,7,7,10a-tetramethyl-1-oxo-3-vinyl-dodecahydro-benzo[f]chromen-5-yl ester

Guidance literature:

With dicyclohexyl-carbodiimide; In 1,4-dioxane; for 2h;

DOI:10.1016/S0040-4039(00)98057-2

upstream raw materials:

4-nitro-phenol

ethylenediamine