Dibutyl-diphenyl-germane

Base Information

Chemical Name:Dibutyl-diphenyl-germane
CAS No.:2848-64-8
Molecular Formula:C₂₀H₂₈Ge
Molecular Weight:341.032
Hs Code.:

Synonyms:

Suppliers and Price of Dibutyl-diphenyl-germane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Dibutyl-diphenyl-germane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Dibutyl-diphenyl-germane

There total 3 articles about Dibutyl-diphenyl-germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.6%

: 100184-59-6
diphenylgermylenedipotassium

: 1675-58-7
diphenylgermane

: 2945-38-2
Butyl-diphenyl-germane

: 2848-64-8
Dibutyl-diphenyl-germane

Guidance literature:: With 1-bromo-butane; water; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; soln. of Ph2GeK2 in HMPA/THF added to n-BuBr, stirred at room temp. for30 min, cooled with water bath, hydrolyzed; extd. with ether, org. layer dried over anhyd. Na2SO4, isolated by preparative GLC and TLC;
DOI:10.1246/bcsj.58.1443

Reference yield: 25.6%

: 109-65-9
1-bromo-butane

: (diphenylgermylene)dipotassium

: 2945-38-2
Butyl-diphenyl-germane

: 2848-64-8
Dibutyl-diphenyl-germane

Guidance literature:: In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; for 0.5h; Product distribution; Ambient temperature;
DOI:10.1246/bcsj.58.1443

Reference yield:

: 132717-10-3
bis-(2,4,6-tri-t-butylphenylamino)diphenylgermane

: 1613-66-7
dichlorodiphenylgermane

: 132717-13-6
di(tri-tert-butylphenyl)-1,3-tetraphenylcyclodigermazane

: 2848-64-8
Dibutyl-diphenyl-germane

Guidance literature:: With n-butyllithium; In benzene; byproducts: LiCl; BuLi in hexane added to amine in benzene, stirred (2h, 45.degreeC, then 17h, 20°C), Ph2GeCl2 added, 8h, 80°C; LiCl filtered off;