1‐(1‐ferrocenylethyl)benzimidazole

Base Information

Chemical Name:1‐(1‐ferrocenylethyl)benzimidazole
CAS No.:810659-33-7
Molecular Formula:C₁₉H₁₈FeN₂
Molecular Weight:330.212
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1‐(1‐ferrocenylethyl)benzimidazole

Chemical Property:

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Technology Process of 1‐(1‐ferrocenylethyl)benzimidazole

There total 3 articles about 1‐(1‐ferrocenylethyl)benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 810659-32-6,521943-91-9
2-(α-ferrocenylethyl)indazole

: 1271-51-8
vinyl ferrocene

: 810659-33-7,521943-89-5
1‐(1‐ferrocenylethyl)benzimidazole

Guidance literature:: In tetrahydrofuran; placing of (C5H5)Fe(C5H4CH(CH3)C7H5N2) in one-neck flask, addn. of THF, reflux for 15 h in air; cooling, chromy. using dimethyl ether as eluent;
DOI:10.1023/A:1021360704054

Reference yield:

: 271-44-3
benzimidazole

: 193092-86-3
1-(α-ferrocenylethyl)-1,2,4-triazole

: 1271-51-8
vinyl ferrocene

: 810659-33-7,521943-89-5
1‐(1‐ferrocenylethyl)benzimidazole

Guidance literature:: With HCl; NH₃; In methanol; water; dissoving of (C5H5)Fe(C5H4CH(CH3)C2H2N3) in methanol on heating; addn. of soln. of indazole in H2O and concd. HCl; reflux for 2.5 h, cooling, neutralizing with aq. ammonia; extn. with dimethyl ether, sepn. of org. layer; monitoring by mass-spectroscopy and comparative chromy. on Silufol plate;
DOI:10.1023/A:1021360704054

Reference yield:

: 288-88-0
1,2,4-Triazole

: 810659-32-6,521943-91-9
2-(α-ferrocenylethyl)indazole

: 1271-51-8
vinyl ferrocene

: 193092-86-3
1-(α-ferrocenylethyl)-1,2,4-triazole

: 810659-33-7,521943-89-5
1‐(1‐ferrocenylethyl)benzimidazole

Guidance literature:: With HCl; NH₃; In ethanol; water; byproducts: C7H6N2; dissolving of (C5H5)Fe(C5H4CH(CH3)C7H5N2) in ethanol on heating, addn. of soln. of 1,2,4-triazole in H2O and concd. HCl; reflux for 2.5 h, cooling, neutralizing with aq. ammonia; extn. with dimethyl ether; sepn. of org layer, TLC chromy. using hexane,benzene and then methanol as eluents;
DOI:10.1023/A:1021360704054