C₆₀H₉₄N₂₀O₁₁S

Base Information

Chemical Name:C₆₀H₉₄N₂₀O₁₁S
CAS No.:716346-07-5
Molecular Formula:C₆₀H₉₄N₂₀O₁₁S
Molecular Weight:1303.6
Hs Code.:

C<sub>60</sub>H<sub>94</sub>N<sub>20</sub>O<sub>11</sub>S

Synonyms:

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Chemical Property of C₆₀H₉₄N₂₀O₁₁S

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Technology Process of C₆₀H₉₄N₂₀O₁₁S

There total 9 articles about C₆₀H₉₄N₂₀O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51673-59-7
1-(2-nitrophenyl)ethane-1,2-diol

: 716346-07-5
C₆₀H₉₄N₂₀O₁₁S

Guidance literature:: Multi-step reaction with 9 steps

1.1: 98.2 percent / thionyl chloride; triethylamine / CH₂Cl₂ / 0.5 h / cooling

2.1: 92.5 percent / sodium azide / dimethylformamide / 2 h / 60 °C

3.1: 91 percent / triphenylphosphine / tetrahydrofuran; H₂O / 1 h / 70 °C

4.1: 99.6 percent / triethylamine / methanol / 2 h

5.1: 98 percent / pyridine / 8 h / 20 °C

6.1: 98 percent / caesium carbonate / dimethylformamide / 24 h

7.1: hydroxylamine / methanol; H₂O / 2 h / pH 6.5

8.1: 95 percent / TFA / 0.5 h

9.1: DIC / CH₂Cl₂

9.2: diisopropylethylamine / dimethylformamide / 12 h

9.3: acid; scavenger

With pyridine; thionyl chloride; sodium azide; hydroxylamine; caesium carbonate; dacarbazine; triethylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 3.1: Staudinger reduction;
DOI:10.1016/j.bmc.2004.02.039

Reference yield:

: 716345-81-2
[2-hydroxy-1-(2-nitro-phenyl)-ethyl]-carbamic acid tert-butyl ester

: 716346-07-5
C₆₀H₉₄N₂₀O₁₁S

Guidance literature:: Multi-step reaction with 5 steps

1.1: 98 percent / pyridine / 8 h / 20 °C

2.1: 98 percent / caesium carbonate / dimethylformamide / 24 h

3.1: hydroxylamine / methanol; H₂O / 2 h / pH 6.5

4.1: 95 percent / TFA / 0.5 h

5.1: DIC / CH₂Cl₂

5.2: diisopropylethylamine / dimethylformamide / 12 h

5.3: acid; scavenger

With pyridine; hydroxylamine; caesium carbonate; dacarbazine; trifluoroacetic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.02.039

Reference yield:

: 716345-87-8
[2-mercapto-1-(2-nitro-phenyl)-ethyl]-carbamic acid tert-butyl ester

: 716346-07-5
C₆₀H₉₄N₂₀O₁₁S

Guidance literature:: Multi-step reaction with 2 steps

1.1: 95 percent / TFA / 0.5 h

2.1: DIC / CH₂Cl₂

2.2: diisopropylethylamine / dimethylformamide / 12 h

2.3: acid; scavenger

With dacarbazine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2004.02.039