(N,N'-di(2.6-diisopropylphenyl)-1,3-propanediamido)titanium dimethyl

Base Information

• Chemical Name: (N,N'-di(2.6-diisopropylphenyl)-1,3-propanediamido)titanium dimethyl
• CAS No.: 179612-35-2
• Molecular Formula: C₂₉H₄₆N₂Ti
• Molecular Weight: 470.578

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Chemical Property of (N,N'-di(2.6-diisopropylphenyl)-1,3-propanediamido)titanium dimethyl

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Technology Process of (N,N'-di(2.6-diisopropylphenyl)-1,3-propanediamido)titanium dimethyl

There total 1 articles about (N,N'-di(2.6-diisopropylphenyl)-1,3-propanediamido)titanium dimethyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

(C6H3(CH(CH3)2)2NCH2)2CH2TiCl2 (179612-33-0) + methylmagnesium bromide (75-16-1) → (N,N'-di(2.6-diisopropylphenyl)-1,3-propanediamido)titanium dimethyl (179612-35-2)

Guidance literature:

In diethyl ether; (N2); Mg compd. dropwise addn. to stirring Ti-compd. soln. (-20°C), warming to room temp., stirring overnight; solvent removal (vac.), solid extraction (hexanes), filtration (Celite),soln. concentrating, cooling (-30°C); elem anal.;

DOI:10.1016/S1381-1169(97)00174-X

Reference yield: 99.0%

(N,N'-di(2.6-diisopropylphenyl)-1,3-propanediamido)titanium dimethyl (179612-35-2) + tris(pentafluorophenyl)borate (1109-15-5) → (CH3)Ti((NC6H3(CH(CH3)2)2)2(CH2)3)(1+)*CH3B(C6F5)3(1-)=[(CH3)Ti((NC6H3(CH(CH3)2)2)2(CH2)3)][CH3B(C6F5)3] (188485-37-2)

Guidance literature:

In pentane; N2-atmosphere, 23°C;

DOI:10.1021/om961034b

Reference yield: 83.0%

(N,N'-di(2.6-diisopropylphenyl)-1,3-propanediamido)titanium dimethyl (179612-35-2) + tris(pentafluorophenyl)borate (1109-15-5) → (C6F5)Ti((NC6H3(CH(CH3)2)2)2(CH2)3)CH2B(C6F5)2

Guidance literature:

In pentane; N2-atmosphere; stirring (23°C, 16 h); filtering, crystn. on concg. (-30°C); elem. anal.;

DOI:10.1021/om961034b

upstream raw materials:

(C₆H₃(CH(CH₃)2)2NCH₂)2CH₂TiCl₂

methylmagnesium bromide

Downstream raw materials:

(CH₃)Ti((NC₆H₃(CH(CH₃)2)2)2(CH₂)3)⁽¹⁺⁾*CH₃B(C₆F₅)3^(1-)=[(CH₃)Ti((NC₆H₃(CH(CH₃)2)2)2(CH₂)3)][CH₃B(C₆F₅)3]

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