(C₅H₅)NiCo(CO)3((C₆H₅)C₂(CH₃))

Base Information

Chemical Name:(C₅H₅)NiCo(CO)3((C₆H₅)C₂(CH₃))
CAS No.:72347-02-5
Molecular Formula:C₁₇H₁₃CoNiO₃
Molecular Weight:382.972
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)NiCo(CO)3((C<sub>6</sub>H<sub>5</sub>)C<sub>2</sub>(CH<sub>3</sub>))

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (C₅H₅)NiCo(CO)3((C₆H₅)C₂(CH₃))

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Technology Process of (C₅H₅)NiCo(CO)3((C₆H₅)C₂(CH₃))

There total 1 articles about (C₅H₅)NiCo(CO)3((C₆H₅)C₂(CH₃)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 1271-28-9
nickelocene

: 53556-74-4
cobalt(carbonyl)3(μ-PhC2Me)cobalt(carbonyl)3

: 72347-02-5
(C₅H₅)NiCo(CO)3((C₆H₅)C₂(CH₃))

Guidance literature:: In hexane; excess Co2(CO)6(PMA), refluxed for 20 h under dry nitrogen gas; chromy. on Florisil, removal of solvent in vac.;

Reference yield:

: 16406-48-7
ruthenium pentacarbonyl

: 72347-02-5
(C₅H₅)NiCo(CO)3((C₆H₅)C₂(CH₃))

: 101316-11-4
(C₅H₅)NiCoRu(CO)6((CH₃)C₂(C₆H₅))

Guidance literature:: In hexane; byproducts: Ru3(CO)12; (N2), excess of Ru(CO)5 and CpNiCo(CO)3(PhC2Me) added to hexane; stirred for 18 h at room temp.; warmed to 40-45°C to decrease reaction time; solvent and excess Ru(CO)5 removed in vacuo; chromd. (Florisil, hexane); eluted (hexane/CH2Cl2); mixture with rotamer in lower yield on behalf of rotating alkyne moiety on face of metal triangle;

Reference yield:

: 16406-49-8,213555-74-9
osmium pentacarbonyl

: 72347-02-5
(C₅H₅)NiCo(CO)3((C₆H₅)C₂(CH₃))

: 101316-12-5
(C₅H₅)NiCoOs(CO)6((CH₃)C₂(C₆H₅))

Guidance literature:: In hexane; byproducts: Os3(CO)12; (N2), excess of Os(CO)5 and CpNiCo(CO)3(PhC2Me) added to hexane; heatedfor 10-12 h to 40-45°C; chromd. (Florisil); eluted (hexane, hexane/CHCl3); rotamer also presenton behalf of rotating alkyne moiety on face of metal triangle;