3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, bis[(2,2-dimethyl-1-oxopropoxy)methyl] ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, bis[(2,2-dimethyl-1-oxopropoxy)methyl] ester
CAS No.:138279-16-0
Molecular Formula:C27H34N2O10
Molecular Weight:546.574
Hs Code.:
Mol file:138279-16-0.mol

Synonyms:

Suppliers and Price of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, bis[(2,2-dimethyl-1-oxopropoxy)methyl] ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, bis[(2,2-dimethyl-1-oxopropoxy)methyl] ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, bis[(2,2-dimethyl-1-oxopropoxy)methyl] ester

There total 4 articles about 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, bis[(2,2-dimethyl-1-oxopropoxy)methyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18997-19-8
Chloromethyl pivalate

: 74936-81-5
1,4-dihydro-2,6-dimethyl-4-(3'-nitrophenyl)-pyridine-3,5-dicarboxylic acid

: 138279-16-0
bis(pivaloyloxymethyl) 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 0 deg C, 30 min, 2.) DMF, RT, 18 h;
DOI:10.1248/cpb.45.863

Reference yield:

: 18997-19-8
Chloromethyl pivalate

: 138279-16-0
bis(pivaloyloxymethyl) 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / dimethylformamide

2: 1 M hydrochloric acid

With hydrogenchloride; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)93560-3

Reference yield:

: 123973-70-6
1,4-dihydro-2,6-dimethyl-1-methoxymethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylic acid

: 138279-16-0
bis(pivaloyloxymethyl) 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / dimethylformamide

2: 1 M hydrochloric acid

With hydrogenchloride; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)93560-3