N-<2-(4-monomethoxytrityl)aminoethyl>aminomethyldiphenyl phosphonate

Base Information

• Chemical Name: N-<2-(4-monomethoxytrityl)aminoethyl>aminomethyldiphenyl phosphonate
• CAS No.: 203643-15-6
• Molecular Formula: C₃₅H₃₅N₂O₄P
• Molecular Weight: 578.648

Synonyms:

Chemical Property of N-<2-(4-monomethoxytrityl)aminoethyl>aminomethyldiphenyl phosphonate

Chemical Property:

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Technology Process of N-<2-(4-monomethoxytrityl)aminoethyl>aminomethyldiphenyl phosphonate

There total 1 articles about N-<2-(4-monomethoxytrityl)aminoethyl>aminomethyldiphenyl phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + diphenyl hydrogen phosphite (4712-55-4) + N1-((4-methoxyphenyl)diphenylmethyl)ethane-1,2-diamine (114729-69-0) → N-<2-(4-monomethoxytrityl)aminoethyl>aminomethyldiphenyl phosphonate (203643-15-6)

Guidance literature:

DOI:10.1080/07328319808004700

Reference yield:

N-<2-(4-monomethoxytrityl)aminoethyl>aminomethyldiphenyl phosphonate (203643-15-6) → {[[2-(6-Benzoylamino-purin-9-yl)-acetyl]-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-methyl}-phosphonic acid 4-methoxy-1-oxy-pyridin-2-ylmethyl ester phenyl ester

Guidance literature:

Multi-step reaction with 3 steps

1: PPh₃ / CCl₄

2: DBU

3: TPSNT

With 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole; triphenylphosphine; In tetrachloromethane;

DOI:10.1080/07328319808004700

Reference yield:

N-<2-(4-monomethoxytrityl)aminoethyl>aminomethyldiphenyl phosphonate (203643-15-6) → C43H39N7O6P(1-)

Guidance literature:

Multi-step reaction with 2 steps

1: PPh₃ / CCl₄

2: DBU

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; In tetrachloromethane;

DOI:10.1080/07328319808004700

upstream raw materials:

formaldehyd

diphenyl hydrogen phosphite

N¹-((4-methoxyphenyl)diphenylmethyl)ethane-1,2-diamine

Downstream raw materials:

({(2-{[(4-Methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-methyl)-phosphonic acid diphenyl ester

{[[2-(6-Benzoylamino-purin-9-yl)-acetyl]-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-methyl}-phosphonic acid diphenyl ester

{[[2-(2-Isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-acetyl]-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-methyl}-phosphonic acid diphenyl ester

{[[2-(4-Benzoylamino-2-oxo-2H-pyrimidin-1-yl)-acetyl]-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-methyl}-phosphonic acid diphenyl ester

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