Methanesulfonic acid (S)-2-{2-[2-((S)-1-methanesulfonyloxymethyl-2,2-dimethyl-propylcarbamoyl)-phenylamino]-benzoylamino}-3,3-dimethyl-butyl ester

Base Information

• Chemical Name: Methanesulfonic acid (S)-2-{2-[2-((S)-1-methanesulfonyloxymethyl-2,2-dimethyl-propylcarbamoyl)-phenylamino]-benzoylamino}-3,3-dimethyl-butyl ester
• CAS No.: 1027046-68-9
• Molecular Formula: C₂₈H₄₁N₃O₈S₂
• Molecular Weight: 611.781

Synonyms:

Chemical Property of Methanesulfonic acid (S)-2-{2-[2-((S)-1-methanesulfonyloxymethyl-2,2-dimethyl-propylcarbamoyl)-phenylamino]-benzoylamino}-3,3-dimethyl-butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of Methanesulfonic acid (S)-2-{2-[2-((S)-1-methanesulfonyloxymethyl-2,2-dimethyl-propylcarbamoyl)-phenylamino]-benzoylamino}-3,3-dimethyl-butyl ester

There total 3 articles about Methanesulfonic acid (S)-2-{2-[2-((S)-1-methanesulfonyloxymethyl-2,2-dimethyl-propylcarbamoyl)-phenylamino]-benzoylamino}-3,3-dimethyl-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanesulfonyl chloride (124-63-0) + 2,2'-bis[N-(1S)-(1-tert-butyl-2-hydroxyethyl)carbamoyl]diphenylamine (815575-19-0) → Methanesulfonic acid (S)-2-{2-[2-((S)-1-methanesulfonyloxymethyl-2,2-dimethyl-propylcarbamoyl)-phenylamino]-benzoylamino}-3,3-dimethyl-butyl ester (1027046-68-9)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 20h;

DOI:10.1016/j.tetasy.2004.09.011

Reference yield:

(S)-tert-leucinol (112245-13-3) → Methanesulfonic acid (S)-2-{2-[2-((S)-1-methanesulfonyloxymethyl-2,2-dimethyl-propylcarbamoyl)-phenylamino]-benzoylamino}-3,3-dimethyl-butyl ester (1027046-68-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / Et₃N / CH₂Cl₂ / 24 h / 20 °C

2: Et₃N / CH₂Cl₂ / 20 h / 20 °C

With triethylamine; In dichloromethane;

DOI:10.1016/j.tetasy.2004.09.011

Reference yield:

Vanadox (579-92-0) → Methanesulfonic acid (S)-2-{2-[2-((S)-1-methanesulfonyloxymethyl-2,2-dimethyl-propylcarbamoyl)-phenylamino]-benzoylamino}-3,3-dimethyl-butyl ester (1027046-68-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / Et₃N / CH₂Cl₂ / 24 h / 20 °C

2: Et₃N / CH₂Cl₂ / 20 h / 20 °C

With triethylamine; In dichloromethane;

DOI:10.1016/j.tetasy.2004.09.011

upstream raw materials:

methanesulfonyl chloride

2,2'-bis[N-(1S)-(1-tert-butyl-2-hydroxyethyl)carbamoyl]diphenylamine

(S)-tert-leucinol

Vanadox

Downstream raw materials:

bis-[2-((4S)-4-tert-butyl-4,5-dihydro-oxazol-2-yl)-phenyl]-amine

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