sodium triethyl(phenylethinyl)borate

Base Information

Chemical Name:sodium triethyl(phenylethinyl)borate
CAS No.:14515-93-6
Molecular Formula:C₁₄H₂₀B*Na
Molecular Weight:222.114
Hs Code.:

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Suppliers and Price of sodium triethyl(phenylethinyl)borate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sodium triethyl(phenylethinyl)borate

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Technology Process of sodium triethyl(phenylethinyl)borate

There total 1 articles about sodium triethyl(phenylethinyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: sodium triethylborohydride

: 536-74-3
phenylacetylene

: 14515-93-6
sodium triethyl(phenylethinyl)borate

Guidance literature:

Reference yield: 68.0%

: 5314-83-0
diethylchloroborane

: 14515-93-6
sodium triethyl(phenylethinyl)borate

: 138517-73-4
(C₂H₅)2BC(C₆H₅)C(C₂H₅)B(C₂H₅)2

Guidance literature:: In diethyl ether; byproducts: NaCl; dropping ClB(C2H5)2 to soln. of Na-salt in diethyl ether within 2 h under Ar, rise in temp. with pptn. of NaCl; refluxing for 5 h; after method of R. Koester, Pure Appl. Chem. 1977, 49, 765-789 and 6 further publications;; filtration; reduction of volume in vac. at <=60°C; distn. in vac.; elem. anal.;;

Reference yield: 34.0%

: 75-77-4
chloro-trimethyl-silane

: 14515-93-6
sodium triethyl(phenylethinyl)borate

: 125212-51-3
(E)-2-diethylboryl-1-phenyl-1-trimethylsilyl-1-butene

Guidance literature:: In diethyl ether; byproducts: NaCl; addn. of Me3SiCl to a soln. of Na(Et3BCCPh), 5 h boiling, filtration, solvent removed (760 Torr, than 14 Torr and < 70°C), distillation at 0.001 Torr; elem. anal.;