C₂₂H₂₇FN₄O₅S

Base Information

Chemical Name:C₂₂H₂₇FN₄O₅S
CAS No.:1416273-10-3
Molecular Formula:C₂₂H₂₇FN₄O₅S
Molecular Weight:478.545
Hs Code.:

C<sub>22</sub>H<sub>27</sub>FN<sub>4</sub>O<sub>5</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₇FN₄O₅S

Chemical Property:

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Technology Process of C₂₂H₂₇FN₄O₅S

There total 6 articles about C₂₂H₂₇FN₄O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1001398-62-4
1-methylethyl 4-{[7-(4-bromo-3-fluorophenyl)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidin-4-yl]oxy}-1-piperidinecarboxylate

: 20277-69-4
sodium methansulfinate

: 1416273-10-3
C₂₂H₂₇FN₄O₅S

Guidance literature:: With copper(l) iodide; L-proline; sodium hydroxide; In dimethyl sulfoxide; at 110 ℃; for 18h; Sealed tube;
DOI:10.1021/jm301404a

Reference yield:

: 16019-30-0
6-hydroxy-5-(2-propen-1-yl)-4(1H)-pyrimidinone

: 1416273-10-3
C₂₂H₂₇FN₄O₅S

Guidance literature:: Multi-step reaction with 6 steps

1.1: trichlorophosphate / 4 h / Inert atmosphere; Reflux

2.1: potassium osmate(VI) dihydrate; sodium periodate / water; acetone / 4 h / 20 °C

3.1: sodium cyanoborohydride; acetic acid / methanol / 19 h / -15 - 20 °C

4.1: potassium tert-butylate / tetrahydrofuran / 22 h / 20 °C

5.1: sodium hydride / tetrahydrofuran / 0.5 h / Reflux

5.2: 1.5 h / 20 °C / Reflux

6.1: copper(l) iodide; L-proline; sodium hydroxide / dimethyl sulfoxide / 18 h / 110 °C / Sealed tube

With potassium osmate(VI) dihydrate; sodium periodate; copper(l) iodide; potassium tert-butylate; sodium hydride; sodium cyanoborohydride; acetic acid; L-proline; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; water; dimethyl sulfoxide; acetone;
DOI:10.1021/jm301404a

Reference yield:

: 16019-31-1
5-allyl-4,6-dichloropyrimidine

: 1416273-10-3
C₂₂H₂₇FN₄O₅S

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium osmate(VI) dihydrate; sodium periodate / water; acetone / 4 h / 20 °C

2.1: sodium cyanoborohydride; acetic acid / methanol / 19 h / -15 - 20 °C

3.1: potassium tert-butylate / tetrahydrofuran / 22 h / 20 °C

4.1: sodium hydride / tetrahydrofuran / 0.5 h / Reflux

4.2: 1.5 h / 20 °C / Reflux

5.1: copper(l) iodide; L-proline; sodium hydroxide / dimethyl sulfoxide / 18 h / 110 °C / Sealed tube

With potassium osmate(VI) dihydrate; sodium periodate; copper(l) iodide; potassium tert-butylate; sodium hydride; sodium cyanoborohydride; acetic acid; L-proline; sodium hydroxide; In tetrahydrofuran; methanol; water; dimethyl sulfoxide; acetone;
DOI:10.1021/jm301404a