3,4-dichlorophenylmercury bromide

Base Information

• Chemical Name: 3,4-dichlorophenylmercury bromide
• CAS No.: 79175-37-4
• Molecular Formula: C₆H₃BrCl₂Hg
• Molecular Weight: 426.49
• Mol file: 79175-37-4.mol

Synonyms:

Chemical Property of 3,4-dichlorophenylmercury bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3,4-dichlorophenylmercury bromide

There total 1 articles about 3,4-dichlorophenylmercury bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

3,4-dichlorophenylmagnesium bromide (79175-35-2) + mercury dibromide → 3,4-dichlorophenylmercury bromide (79175-37-4)

Guidance literature:

With ammonium bromide; In tetrahydrofuran; diethyl ether; soln. of 3,4-Cl2C6H3MgBr in abs. ether added with stirring to soln. of HgBr2 in abs. THF, heated in water bath for 2.5 h, after 12 h at 25°C decompd. with soln. of NH4Br; org. layer sepd. off, driven off in vac., recrystd. (xylene); elem. anal.;

DOI:10.1007/BF00949709

Reference yield: 70.0%

3,4-dichlorophenylmercury bromide (79175-37-4) → Hg(Cl2C6H3)2 (73282-89-0)

Guidance literature:

With hydrazine hydrate; In N,N-dimethyl-formamide; soln. of 3,4-Cl2C6H3HgBr treated with N2H4*99H2O, stirred for 1 h; Hg filtered off, poured into 1 L of destd. water, filtered off, recrystd. (ethanol); elem. anal.;

DOI:10.1007/BF00949709

upstream raw materials:

3,4-dichlorophenylmagnesium bromide

Downstream raw materials:

Hg(Cl₂C₆H₃)2