C₂₉H₃₂OPRu

Base Information

Chemical Name:C₂₉H₃₂OPRu
CAS No.:112861-31-1
Molecular Formula:C₂₉H₃₂OPRu
Molecular Weight:528.616
Hs Code.:

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Chemical Property of C₂₉H₃₂OPRu

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Technology Process of C₂₉H₃₂OPRu

There total 2 articles about C₂₉H₃₂OPRu which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 112861-27-5
RuCl(CO)(P(C₆H₅)3)(C₅(CH₃)5)

: 112861-31-1
(C₅(CH₃)5)RuH(CO)P(C₆H₅)3

Guidance literature:: With methanol; sodium methylate; In methanol; MeONa was added to a suspn. of Ru-complex in MeOH under N2, mixt. was stirred at 50°C for 6 h; evapd., residue was extd. with light petroleum, ext. concd., cooled to -20°C; elem. anal.;
DOI:10.1016/0022-328X(87)85009-X

Reference yield: 61.0%

: 15243-33-1
dodecacarbonyl-triangulo-triruthenium

: 4045-44-7
1,2,3,4,5-pentamethylcyclopentadiene

: 603-35-0
triphenylphosphine

: 112861-31-1
C₂₉H₃₂OPRu

Guidance literature:: dodecacarbonyl-triangulo-triruthenium; 1,2,3,4,5-pentamethylcyclopentadiene; In 1,4-dioxane; at 20 ℃; for 1h; Glovebox; Schlenk technique; Reflux; Inert atmosphere;

triphenylphosphine; In n-heptane; for 2h; Glovebox; Schlenk technique; Reflux; Inert atmosphere;
DOI:10.1021/ja3119477