Pd{bis{o-(methylthio)phenyl}phenylphosphino}Br₂

Base Information

• Chemical Name: Pd{bis{o-(methylthio)phenyl}phenylphosphino}Br₂
• CAS No.: 141446-47-1
• Molecular Formula: C₂₀H₁₉Br₂PPdS₂
• Molecular Weight: 620.705
• Mol file: 141446-47-1.mol

Synonyms:

Chemical Property of Pd{bis{o-(methylthio)phenyl}phenylphosphino}Br₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Pd{bis{o-(methylthio)phenyl}phenylphosphino}Br₂

There total 1 articles about Pd{bis{o-(methylthio)phenyl}phenylphosphino}Br₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

potassium tetrachloropalladate(II) (10025-98-6) + bis-(2-methylthiophenyl)-phenylphosphine (14791-95-8) + lithium bromide (7550-35-8) → Pd{bis{o-(methylthio)phenyl}phenylphosphino}Br2 (141446-47-1)

Guidance literature:

In water; acetone; Schlenk procedure; method of S. E. Livingstone and T. N. Lockyer, Inorg. Nucl. Chem. Lett., 1967, 3, 35 was adopted: addn. of excess LiBr to boiling acetone soln. of phosphine, addn. of Pd-complex in distd. H2O, pptn.; filtration, washed (hexane); elem. anal.;

DOI:10.1039/DT9920001073

upstream raw materials:

potassium tetrachloropalladate(II)

bis-(2-methylthiophenyl)-phenylphosphine

lithium bromide