tris(diphenylstibino)amine

Base Information

• Chemical Name: tris(diphenylstibino)amine
• CAS No.: 408514-86-3
• Molecular Formula: C₃₆H₃₀NSb₃
• Molecular Weight: 841.891
• Mol file: 408514-86-3.mol

Synonyms:

Chemical Property of tris(diphenylstibino)amine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of tris(diphenylstibino)amine

There total 1 articles about tris(diphenylstibino)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.5%

ammonia (7664-41-7) + diphenylantimony(III) chloride (2629-47-2) → tris(diphenylstibino)amine (408514-86-3)

Guidance literature:

In ammonia; byproducts: NH4Cl; NH3 (liquid); all manipulations under Ar; Sb compd. added to liq. NH3 at -70°C with stirring, stirred at -70°C for 1 h, then stirred without cooling for 24 h; residue of NH3 removed in vac., (Ph2Sb)3N dissolved in toluene, solvent evapd. in vac., compd. washed with petroleum ether; elem. anal.;

DOI:10.1515/znb-2001-1213

upstream raw materials:

ammonia

diphenylantimony(III) chloride