methyl 3-(5-methylpyridin-3-yl)-5-(methylsulfonyl)benzoate

Base Information

Chemical Name:methyl 3-(5-methylpyridin-3-yl)-5-(methylsulfonyl)benzoate
CAS No.:1186519-02-7
Molecular Formula:C₁₅H₁₅NO₄S
Molecular Weight:305.354
Hs Code.:

Synonyms:

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Chemical Property of methyl 3-(5-methylpyridin-3-yl)-5-(methylsulfonyl)benzoate

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Technology Process of methyl 3-(5-methylpyridin-3-yl)-5-(methylsulfonyl)benzoate

There total 3 articles about methyl 3-(5-methylpyridin-3-yl)-5-(methylsulfonyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 618-58-6
3,5-dibromobenzoic acid

: 1186519-02-7
methyl 3-(5-methylpyridin-3-yl)-5-(methylsulfonyl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethyl sulfoxide / 4 h / 100 °C / Sealed tube

2.1: Chloro-oxo-acetic acid; N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C

2.2: 3 h / 20 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

With Chloro-oxo-acetic acid; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; dimethyl sulfoxide; toluene;

Reference yield:

: 453566-01-3
methyl 3-bromo-5-(methylthio)benzoate

: 1186519-02-7
methyl 3-(5-methylpyridin-3-yl)-5-(methylsulfonyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

With 3-chloro-benzenecarboperoxoic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; toluene;

Reference yield:

: 453566-00-2
3-bromo-5-methylsulfanylbenzoic acid

: 1186519-02-7
methyl 3-(5-methylpyridin-3-yl)-5-(methylsulfonyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: Chloro-oxo-acetic acid; N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C

1.2: 3 h / 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

With Chloro-oxo-acetic acid; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; toluene;