2-(1,3-Dioxo-2-p-tolyl-2,3-dihydro-1H-benzo[de]isoquinolin-6-yl)-2H-naphtho[1,2-d][1,2,3]triazole-5-sulfonic acid methylamide

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Chemical Name:2-(1,3-Dioxo-2-p-tolyl-2,3-dihydro-1H-benzo[de]isoquinolin-6-yl)-2H-naphtho[1,2-d][1,2,3]triazole-5-sulfonic acid methylamide
CAS No.:106498-15-1
Molecular Formula:C₃₀H₂₁N₅O₄S
Molecular Weight:547.594
Hs Code.:

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Chemical Property of 2-(1,3-Dioxo-2-p-tolyl-2,3-dihydro-1H-benzo[de]isoquinolin-6-yl)-2H-naphtho[1,2-d][1,2,3]triazole-5-sulfonic acid methylamide

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Technology Process of 2-(1,3-Dioxo-2-p-tolyl-2,3-dihydro-1H-benzo[de]isoquinolin-6-yl)-2H-naphtho[1,2-d][1,2,3]triazole-5-sulfonic acid methylamide

There total 5 articles about 2-(1,3-Dioxo-2-p-tolyl-2,3-dihydro-1H-benzo[de]isoquinolin-6-yl)-2H-naphtho[1,2-d][1,2,3]triazole-5-sulfonic acid methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84-86-6
4-amino-1-naphthalenesufonic acid

: 106498-15-1
2-(1,3-Dioxo-2-p-tolyl-2,3-dihydro-1H-benzo[de]isoquinolin-6-yl)-2H-naphtho[1,2-d][1,2,3]triazole-5-sulfonic acid methylamide

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) nitrosylsulphuric acid, 2.) sodium carbonate / 2.) H₂O, 0-10 deg C, pH 6-6.5, 5h

2: 89.1 percent / cupric acetate, air / dimethylformamide / 0.75 h / 90 °C

3: 78 percent / thionyl chloride, DMF / chlorobenzene / 60 deg C, 1h; 95 deg C, 2h

4: dimethylformamide

With thionyl chloride; nitrosylsulfuric acid; air; copper diacetate; sodium carbonate; N,N-dimethyl-formamide; In N,N-dimethyl-formamide; chlorobenzene;

Reference yield:

: 20871-08-3
4-amino-N-(p-tolyl)naphthalimide

: 106498-15-1
2-(1,3-Dioxo-2-p-tolyl-2,3-dihydro-1H-benzo[de]isoquinolin-6-yl)-2H-naphtho[1,2-d][1,2,3]triazole-5-sulfonic acid methylamide

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) nitrosylsulphuric acid, 2.) sodium carbonate / 2.) H₂O, 0-10 deg C, pH 6-6.5, 5h

2: 89.1 percent / cupric acetate, air / dimethylformamide / 0.75 h / 90 °C

3: 78 percent / thionyl chloride, DMF / chlorobenzene / 60 deg C, 1h; 95 deg C, 2h

4: dimethylformamide

With thionyl chloride; nitrosylsulfuric acid; air; copper diacetate; sodium carbonate; N,N-dimethyl-formamide; In N,N-dimethyl-formamide; chlorobenzene;

Reference yield:

: 106450-39-9
4-(5-sulpho-2H-naphtho<1,2-d>triazol-2-yl)-N-(p-tolyl)naphthalimide

: 106498-15-1
2-(1,3-Dioxo-2-p-tolyl-2,3-dihydro-1H-benzo[de]isoquinolin-6-yl)-2H-naphtho[1,2-d][1,2,3]triazole-5-sulfonic acid methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / thionyl chloride, DMF / chlorobenzene / 60 deg C, 1h; 95 deg C, 2h

2: dimethylformamide

With thionyl chloride; N,N-dimethyl-formamide; In N,N-dimethyl-formamide; chlorobenzene;