C₁₆H₂₁N₂O₂PS

Base Information

Chemical Name:C₁₆H₂₁N₂O₂PS
CAS No.:127136-66-7
Molecular Formula:C₁₆H₂₁N₂O₂PS
Molecular Weight:336.395
Hs Code.:

C<sub>16</sub>H<sub>21</sub>N<sub>2</sub>O<sub>2</sub>PS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₂₁N₂O₂PS

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Technology Process of C₁₆H₂₁N₂O₂PS

There total 2 articles about C₁₆H₂₁N₂O₂PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 7393-13-7
(1-phenyl)-N,N,N',N'-tetramethyldiamido phosphate

: 882-33-7
diphenyldisulfane

: 127136-66-7
C₁₆H₂₁N₂O₂PS

Guidance literature:: With sec.-butyllithium; 1.) cyclohexane, THF, -105 deg C, 1 h, 2.) cyclohexane, THF, -105 deg C, 1 h;
DOI:10.1248/cpb.38.2637

Reference yield:

: 108-95-2,27073-41-2
phenol

: 127136-66-7
C₁₆H₂₁N₂O₂PS

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 1.) NaH / 1.) THF, 30 min, room temperature, 2.) THF, 12 h, room temperature

2: 64 percent / 1.) sec-BuLi / 1.) cyclohexane, THF, -105 deg C, 1 h, 2.) cyclohexane, THF, -105 deg C, 1 h

With sec.-butyllithium; sodium hydride;
DOI:10.1248/cpb.38.2637