b-D-Glucopyranosiduronic acid, (3b,16a,21b,22a)-16,21,22,28-tetrahydroxyolean-12-en-3-ylO-6-deoxy-a-L-mannopyranosyl-(1®2)-O-b-D-galactopyranosyl-(1®3)-O-[b-D-glucopyranosyl-(1®2)]- (9CI)

Base Information

Chemical Name:b-D-Glucopyranosiduronic acid, (3b,16a,21b,22a)-16,21,22,28-tetrahydroxyolean-12-en-3-ylO-6-deoxy-a-L-mannopyranosyl-(1®2)-O-b-D-galactopyranosyl-(1®3)-O-[b-D-glucopyranosyl-(1®2)]- (9CI)
CAS No.:53962-19-9
Molecular Formula:C54H88 O25
Molecular Weight:1137.28
Hs Code.:

b-D-Glucopyranosiduronic acid, (3b,16a,21b,22a)-16,21,22,28-tetrahydroxyolean-12-en-3-ylO-6-deoxy-a-L-mannopyranosyl-(1®2)-O-b-D-galactopyranosyl-(1®3)-O-[b-D-glucopyranosyl-(1®2)]- (9CI)

Synonyms:Oleanane,b-D-glucopyranosiduronic acidderiv.; Deacyljegosaponin; Desacyljegosaponin; Jegosaponin, deacyl-

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Chemical Property of b-D-Glucopyranosiduronic acid, (3b,16a,21b,22a)-16,21,22,28-tetrahydroxyolean-12-en-3-ylO-6-deoxy-a-L-mannopyranosyl-(1®2)-O-b-D-galactopyranosyl-(1®3)-O-[b-D-glucopyranosyl-(1®2)]- (9CI)

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Technology Process of b-D-Glucopyranosiduronic acid, (3b,16a,21b,22a)-16,21,22,28-tetrahydroxyolean-12-en-3-ylO-6-deoxy-a-L-mannopyranosyl-(1®2)-O-b-D-galactopyranosyl-(1®3)-O-[b-D-glucopyranosyl-(1®2)]- (9CI)

There total 3 articles about b-D-Glucopyranosiduronic acid, (3b,16a,21b,22a)-16,21,22,28-tetrahydroxyolean-12-en-3-ylO-6-deoxy-a-L-mannopyranosyl-(1®2)-O-b-D-galactopyranosyl-(1®3)-O-[b-D-glucopyranosyl-(1®2)]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21-O-angeloyl-22-O-acetylbarringtogenol C 3-O-[β-D-glucopyranosyl(1->2)][α-L-rhamnopyranosyl(1->2)-β-D-galactopyranosyl(1->3)]-β-D-glucuronopyranoside

: 565-63-9
Angelic acid

: 53962-19-9
desacyl-jegosaponin

Guidance literature:: With water; potassium hydroxide; In 1,4-dioxane; at 37 ℃; for 6h;
DOI:10.1248/cpb.60.752

Reference yield:

: 1160430-52-3
21,22-di-O-tigloyl barringtogenol 3-O-β-D-glucopyranosyl(1->2)[α-L-rhamnopyranosyl(1->2)-β-D-galactopyranosyl(1->3)]-β-D-glucopyranosiduronic acid

: 80-59-1
Tiglic acid

: 53962-19-9
desacyl-jegosaponin

Guidance literature:: With potassium hydroxide; water; In 1,4-dioxane; at 37 ℃; for 1h;
DOI:10.1248/cpb.57.269

Reference yield:

: 1160430-52-3
21,22-di-O-tigloyl barringtogenol 3-O-β-D-glucopyranosyl(1->2)[α-L-rhamnopyranosyl(1->2)-β-D-galactopyranosyl(1->3)]-β-D-glucopyranosiduronic acid

: 2978-11-2
p-nitrobenzyl-N,N′-diisopropylisourea

: p-nitrobenzyl ester of tiglic acid

: 53962-19-9
desacyl-jegosaponin

Guidance literature:: 21,22-di-O-tigloyl barringtogenol 3-O-β-D-glucopyranosyl(1->2)[α-L-rhamnopyranosyl(1->2)-β-D-galactopyranosyl(1->3)]-β-D-glucopyranosiduronic acid; With potassium hydroxide; water; In 1,4-dioxane; at 37 ℃; for 1h;

p-nitrobenzyl-N,N′-diisopropylisourea; In 1,2-dichloro-ethane; at 80 ℃; for 1h;
DOI:10.1248/cpb.57.269