1,1-bis(2,4-2H6>phenyl)-2-methylpropane

Base Information

• Chemical Name: 1,1-bis(2,4-2H6>phenyl)-2-methylpropane
• CAS No.: 138002-59-2
• Molecular Formula: C₂₀H₂₆O₄
• Molecular Weight: 342.329
• Mol file: 138002-59-2.mol

Synonyms:

Chemical Property of 1,1-bis(2,4-2H6>phenyl)-2-methylpropane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1-bis(2,4-2H6>phenyl)-2-methylpropane

There total 3 articles about 1,1-bis(2,4-2H6>phenyl)-2-methylpropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1,3-bis-trideuteriomethoxybenzene (16469-85-5) + isobutyraldehyde (78-84-2) → 1,1-bis(2,4-2H6>phenyl)-2-methylpropane (138002-59-2)

Guidance literature:

DOI:10.1002/oms.1210261010

Reference yield:

2,4-Dimethoxybenzaldehyde (613-45-6) → 1,1-bis(2,4-2H6>phenyl)-2-methylpropane (138002-59-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.1 g / diethyl ether

2: AcOH, 70percent H₂SO₄ / 24 h / Ambient temperature; other 1-dimethoxy-2-methyl-1-propanols and hexadeutero dimethoxybenzenes

With sulfuric acid; acetic acid; In diethyl ether;

DOI:10.1248/cpb.42.375

Reference yield:

1,3-bis-trideuteriomethoxybenzene (16469-85-5) + 1-(2,4-dimethoxyphenyl)-2-methyl-1-propanol → α,α-bis(2,4-dimethoxyphenyl)-β,β-dimethylethane (85238-99-9) + 1-(2,5-dimethoxyphenyl)-1-(2,5-phenyl)-2-methylpropane (138002-60-5) + 1,1-bis(2,4-2H6>phenyl)-2-methylpropane (138002-59-2)

Guidance literature:

With sulfuric acid; acetic acid; for 24h; Title compound not separated from byproducts; Ambient temperature;

DOI:10.1248/cpb.42.375

upstream raw materials:

1,3-bis-trideuteriomethoxybenzene

isobutyraldehyde

2,4-Dimethoxybenzaldehyde