8-amino-N-(benzyloxy)octanamide

Base Information

Chemical Name:8-amino-N-(benzyloxy)octanamide
CAS No.:1122748-11-1
Molecular Formula:C₁₅H₂₄N₂O₂
Molecular Weight:264.368
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-amino-N-(benzyloxy)octanamide

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Technology Process of 8-amino-N-(benzyloxy)octanamide

There total 4 articles about 8-amino-N-(benzyloxy)octanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 8-azido-N-(benzyloxy)octanamide

: 1122748-11-1
8-amino-N-(benzyloxy)octanamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 2h;
DOI:10.1021/acsmedchemlett.9b00561

Reference yield:

: 217180-76-2
8-azido octanoic acid

: 1122748-11-1
8-amino-N-(benzyloxy)octanamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 2 h / 20 °C

With palladium 10% on activated carbon; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/acsmedchemlett.9b00561

Reference yield:

: 17696-11-6
8-bromooctanoic acid

: 1122748-11-1
8-amino-N-(benzyloxy)octanamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / N,N-dimethyl-formamide / 48 h / 77 °C

2: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 2 h / 20 °C

With sodium azide; palladium 10% on activated carbon; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/acsmedchemlett.9b00561