α-benzenessigsaeure-methylester

Base Information

Chemical Name:α-benzenessigsaeure-methylester
CAS No.:17226-93-6
Molecular Formula:C₁₆H₁₆O₃
Molecular Weight:256.301
Hs Code.:

α-<Hydroxy(phenyl)methyl>benzenessigsaeure-methylester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-benzenessigsaeure-methylester

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Technology Process of α-benzenessigsaeure-methylester

There total 24 articles about α-benzenessigsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 100-52-7
benzaldehyde

: 101-41-7
benzeneacetic acid methyl ester

: 17226-93-6,17226-94-7,58769-52-1,58769-53-2,93434-58-3,120851-53-8,139628-23-2
α-benzenessigsaeure-methylester

Guidance literature:: benzeneacetic acid methyl ester; With triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane; In dichloromethane; at -78 ℃; for 2h; Inert atmosphere;

benzaldehyde; In dichloromethane; at -78 ℃; for 3h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol301782s

Reference yield: 91.0%

: 54108-62-2
3-Oxo-2,3-diphenylpropenoic acid methyl ester

: 17226-93-6,17226-94-7,58769-52-1,58769-53-2,93434-58-3,120851-53-8,139628-23-2
(2R,3R)-und (2S,3S)-3-Hydroxy-2,3-diphenylpropansaeure-methylester

Guidance literature:: With zinc(II) tetrahydroborate; zinc(II) chloride; In diethyl ether; at -15 ℃; for 5h;

Reference yield: 85.0%

: 100-52-7
benzaldehyde

: 101-41-7
benzeneacetic acid methyl ester

: 17226-93-6,17226-94-7,58769-52-1,58769-53-2,93434-58-3,120851-53-8,139628-23-2
(2R,3R)-und (2S,3S)-3-Hydroxy-2,3-diphenylpropansaeure-methylester

Guidance literature:: benzeneacetic acid methyl ester; With di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃;

benzaldehyde; In dichloromethane; at -78 ℃; for 0.75h;
DOI:10.1016/S0040-4039(00)00582-7